Production of levulinic acid from glucosamine using zirconium oxychloride

被引：10
|
作者：
Park, Mi-Ra [1 ]
Kim, Sung-Koo [1 ]
Jeong, Gwi-Taek [1 ]
机构：
[1] Pukyong Natl Univ, Dept Biotechnol, Busan 48513, South Korea
来源：
JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY | 2018年 / 61卷
基金：
新加坡国家研究基金会;
关键词：
Glucosamine; Zirconium oxychloride; Platform chemicals; 5-Hydroxymethylfurfural; Levulinic acid; 5-HYDROXYMETHYLFURFURAL HMF; HYDROTHERMAL PROCESS; DIRECT CONVERSION; CHITIN BIOMASS; CELLULOSE; BIOFUEL; OPPORTUNITIES; CHALLENGES; CHEMICALS; CATALYSTS;
D O I：
10.1016/j.jiec.2017.12.008
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
In this study, we evaluated zirconium oxychloride (ZrOCl2), an eco-friendly Lewis acid as a catalyst for conversion of glucosamine (a monomer of chitosan obtained from shell-crustacean food waste) into levulinic acid (LA). In a ZrOCl2-catalyzed hydrothermal reaction, 21.29 mol% of LA was obtained using Optimized conditions with 50 glucosamine and 15 mol% ZrOCl2, at 200 degrees C for 20 min. Our results demonstrate the potential of glucosamine as a recyclable feedstock and ZrOCl2 as an eco-friendly catalyst for platform chemical synthesis. (C) 2017 The Korean Society of Industrial and Engineering Chemistry. Published by Elsevier B.V. All rights reserved.
引用
收藏
页码：119 / 123
页数：5
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