1,4-Diazabicyclo[2.2.2]octanium 2,4-dinitrophenolate

被引：12

作者：

Chantrapromma, S

Usman, A

Fun, HK ^{[1
]}

Poh, BL

Karalai, C

机构：

[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, George Town 11800, Malaysia

[2] Univ Sains Malaysia, Sch Chem, George Town 11800, Malaysia

[3] Prince Songkla Univ, Fac Sci, Dept Chem, Hat Yai 90112, Songkhla, Thailand

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2002年 / 58卷

关键词：

D O I：

10.1107/S1600536801021791

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title salt, C6H13N2+.C6H3N2O5-, the cation acts as a donor for the bifurcated intermolecular N-H...O hydrogen bonding interactions with the O atoms of the phenolate and one of the nitro groups of the 2,4-dinitrophenolate. The crystal packing structure is built from molecular ribbons of 2,4-dinitrophenolates parallel to the c axis, with the cation linking them by four intermolecular C-H...O hydrogen bonds.

引用

页码：o102 / o104

页数：3

共 12 条

[1]

[Anonymous], 1996, SMART SAINT

[2] Salts of 3,5-dinitrobenzoic acid with organic diamines: hydrogen-bonded supramolecular structures in one, two and three dimensions [J].

Burchell, CJ ;

Glidewell, C ;

Lough, AJ ;

Ferguson, G .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 2001, 57 (02) :201-212

[3] The 1:2 adduct N,N-dimethylethylenediamine-1,4-diium bis(2,4-dinitrophenolate) [J].

Chantrapromma, S ;

Usman, A ;

Fun, HK ;

Poh, BL ;

Karalai, C .

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2002, 58 :o108-o110

[4] GENERAL DEFINITION OF RING PUCKERING COORDINATES [J].

CREMER, D ;

POPLE, JA .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1975, 97 (06) :1354-1358

[5] Chain, sheet and framework structures in the adducts of phenylphosphonic acid with 4,4′-bipyridyl (1/1), piperazine (2/1) and 1,4-diazabicyclo[2.2.2]octane (2/1) [J].

Ferguson, G ;

Glidewell, C ;

Gregson, RM ;

Meehan, PR .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1998, 54 :129-138

[6] Crystal engineering using trisphenols. Three-dimensional hydrogen-bonding networks in 1,1,1-tris(4-hydroxyphenyl)ethane, its hydrated adduct with 1,4-diazabicyclo[2.2.2]octane(1/1/1) and its adduct with piperazine(4/3) [J].

Ferguson, G ;

Bell, W ;

Coupar, PI ;

Glidewell, C .

ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1997, 53 :534-543

[7]

Nardelli M., 1995, J APPL CRYSTALLOGR, V28, P659, DOI [10.1107/S0021889895007138, DOI 10.1107/S0021889895007138]

[8]

Sheldrick G.M., 1996, SADABS VERSION 2008

[9]

Sheldrick G.M., 1997, SHELXTL VERSION 5 1

[10]

Spek A., 1990, ACTA CRYSTALLOGR, V46

← 1 2 →