Rapid determination of 239Pu in urine samples using molecular recognition technology product AnaLigA®Pu-02 gel

被引：0

作者：

Dulanska, Silvia ^{[1
]}

Remenec, Boris ^{[1
]}

Bilohuscin, Jan ^{[1
]}

Labaska, Miroslav ^{[1
]}

Horvathova, Bianka ^{[1
]}

Matel, Andrej ^{[2
]}

机构：

[1] Comenius Univ, Dept Nucl Chem, Fac Nat Sci, Bratislava 84215, Slovakia

[2] Constantine Philosopher Univ, Fac Social Sci & Hlth Care, Nitra 94974, Slovakia

来源：

JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY | 2013年 / 298卷 / 01期

关键词：

Urine analysis; Bioassay; Pre-concentration; Pu-239; EXTRACTION CHROMATOGRAPHY; EMERGENCY URINE; SR-90; SEPARATION; ACTINIDES;

D O I：

10.1007/s10967-013-2457-3

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

This paper describes the use of IBC's AnaLig(A (R))Pu-02 molecular recognition technology product to effectively and selectively pre-concentrate, separate and recover plutonium from urine samples. This method uses two-stage column separations consisting of two different commercial products, Eichrom's Pre-filter Material and AnaLig(A (R))Pu-02 resin from IBC Advanced Technologies. By eliminating the co-precipitation techniques and the ashing steps to remove residual organics, the analysis time was reduced significantly. The method was successfully tested by adding known activities of reference solutions of Pu-242 and Pu-239 to urine samples.

引用

页码：439 / 442

页数：4

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