Structural, Optical and Magnetic Properties of NiO Nanopowders

被引：27
|
作者：
Rani, B. Jansi [1 ]
Saravanakumar, B. [2 ]
Ravi, G. [1 ]
Ganesh, V. [3 ]
Sakunthala, A. [4 ]
Yuvakkumar, R. [1 ]
机构：
[1] Alagappa Univ, Nanomat Lab, Dept Phys, Karaikkudi 630003, Tamil Nadu, India
[2] Chonbuk Natl Univ, Dept Organ Mat & Fiber Engn, Jeonju 561756, South Korea
[3] CSIR Cent Electrochem Res Inst CSIR CECRI, Electrod & Electrocatalysis EEC Div, Karaikkudi 630003, Tamil Nadu, India
[4] Karunya Univ, Sch Sci & Humanities, Dept Phys, Coimbatore 641114, Tamil Nadu, India
来源：
JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY | 2018年 / 18卷 / 07期
关键词：
Cubic NiO; XRD; Raman; TEM; VSM; LI-ION BATTERIES; OXIDE THIN-FILMS; THERMAL-DECOMPOSITION; ELECTRODE MATERIAL; SOLAR-CELLS; NANOPARTICLES; WATER; NANOCRYSTALS; NANORODS; SURFACE;
D O I：
10.1166/jnn.2018.15301
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Nickel oxide (NiO) nanopowders were synthesized without using surfactant by chemical reduction technique. NaBH4 influence on structural, optical and magnetic properties of NiO product was investigated. XRD results revealed the formation of dominant single phase, cubic face centered nickel oxide. Raman peaks depicts the characteristic first-order transverse optical (TO) phonon, two phonon excitation (TO + LO), excitation (2LO) Raman mode vibrations of face centered cubic NiO. PL studies revealed the presence of strong emission band which is in good agreement with the intrinsic NiO product. FTIR studies explored metal oxygen vibrations of the obtained product. TEM results revealed the nanoscale product with spherical shape structures. VSM studies explored weak ferromagnetic behavior of the obtained product. High concentration of NaBH4 increases magnetization value and exhibits the typical weak ferromagnetic curve. Reducing agent played a vital role in the structural, optical and magnetic properties of the obtained NiO product.
引用
收藏
页码：4658 / 4666
页数：9
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