FTIR-evolved gas analysis in recent thermoanalytical investigations

被引:44
作者
Risoluti, Roberta [1 ]
Fabiano, Maria Aurora [1 ]
Gullifa, Giuseppina [1 ]
Ciprioti, Stefano Vecchio [2 ]
Materazzi, Stefano [1 ]
机构
[1] Sapienza Univ Rome, Dept Chem, Piazzale A Moro 5, I-00185 Rome, Italy
[2] Sapienza Univ Rome, Dept Basic & Appl Sci Engn, Rome, Italy
关键词
EGA; EGA-FTIR; evolved gas analysis; infrared spectroscopy; IR; TG-FTIR; TRANSFORM-INFRARED-SPECTROSCOPY; INTUMESCENT FLAME-RETARDANT; THERMAL-DEGRADATION MECHANISM; CHEMICAL LOOPING COMBUSTION; MUNICIPAL SOLID-WASTE; WALLED CARBON NANOTUBES; EGA-MS CHARACTERIZATION; TG-FTIR; PYROLYSIS CHARACTERISTICS; BIOMIMETIC COMPLEXES;
D O I
10.1080/05704928.2016.1207658
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Several analytical instruments (like pyrolyzers, thermobalances, differential thermal analyzers, or calorimeters, and sometimes simply temperature-controlled reactors) can be on-line coupled to infrared spectrometers to perform evolved gas analysis (EGA). Advances in EGA techniques are currently proposed by the scientific literature because the possibility to on-line detect the nature of the released gases or vapors has become fundamental to proving a supposed reaction, either under isothermal or under heating conditions. In this review, recent analytical applications of evolved gas analysis performed by infrared spectroscopy (EGA-IR), selected among those published in the years 2013 to 2015, are collected.
引用
收藏
页码:39 / 72
页数:34
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