Synthesis of surfactant-free self-assembled and size-controlled ZnS mesoporous nanospheres

被引:11
作者
Zhang, Qian [1 ]
Chi, Wenyang [1 ]
Zhang, Weiwei [1 ]
Lv, Chunyan [1 ]
Li, Jixue [1 ]
机构
[1] Jilin Univ, Coll Chem, State Key Lab Inorgan Synth & Preparat Chem, Changchun 130012, Peoples R China
基金
中国国家自然科学基金;
关键词
VISIBLE-LIGHT IRRADIATION; PHOTOCATALYTIC ACTIVITY; GROWTH-MECHANISM; NANOSTRUCTURES; NANOBELTS; PERFORMANCE; NANOWIRES; EVOLUTION; SPHERES;
D O I
10.1039/c1nj20727j
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
High quality self-assembled ZnS mesoporous nanospheres have been successfully synthesized by a facile solvothermal method. The sample was synthesized using ethylene glycol aqueous solution without any surfactant assistance. Size and shape control of the ZnS mesoporous nanospheres is achieved by simple adjustments of the reactants' concentration. Investigation results show that ZnS spheres are made up of small ZnS nanocrystallites and show good photocatalytic activity in the degradation of MB under the irradiation of ultraviolet light because of their mesoporous structures.
引用
收藏
页码:119 / 124
页数:6
相关论文
共 32 条
[11]   Pore size determination in modified micro- and mesoporous materials.: Pitfalls and limitations in gas adsorption data analysis [J].
Groen, JC ;
Peffer, LAA ;
Pérez-Ramírez, J .
MICROPOROUS AND MESOPOROUS MATERIALS, 2003, 60 (1-3) :1-17
[12]   Reduction of nitrate and nitrite ions over Ni-ZnS photocatalyst under visible light irradiation in the presence of a sacrificial reagent [J].
Hamanoi, O ;
Kudo, A .
CHEMISTRY LETTERS, 2002, (08) :838-839
[13]   Mass production and high photocatalytic activity of ZnS nanoporous nanoparticles [J].
Hu, JS ;
Ren, LL ;
Guo, YG ;
Liang, HP ;
Cao, AM ;
Wan, LJ ;
Bai, CL .
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2005, 44 (08) :1269-1273
[14]   Catalytic growth and photoluminescence properties of ZnS nanowires [J].
Kar, S ;
Biswas, S ;
Chaudhuri, S .
NANOTECHNOLOGY, 2005, 16 (06) :737-740
[15]   Photocatalytic H2 evolution under visible light irradiation on Ni-doped ZnS photocatalyst [J].
Kudo, A ;
Sekizawa, M .
CHEMICAL COMMUNICATIONS, 2000, (15) :1371-1372
[16]   Mesoporous ZnS nanospheres: a high activity heterogeneous catalyst for synthesis of 5-substituted 1H-tetrazoles from nitriles and sodium azide [J].
Lang, Leiming ;
Li, Baojun ;
Liu, Wei ;
Jiang, Li ;
Xu, Zheng ;
Yin, Gui .
CHEMICAL COMMUNICATIONS, 2010, 46 (03) :448-450
[17]   Optical, photocatalytic properties of novel CuS nanoplate-based architectures synthesised by a solvothermal route [J].
Li, Fei ;
Bi, Wentuan ;
Kong, Tao ;
Qin, Qinghua .
CRYSTAL RESEARCH AND TECHNOLOGY, 2009, 44 (07) :729-735
[18]   One-pot synthesis of monodispersed ZnS nanospheres with high antibacterial activity [J].
Li, Gaiping ;
Zhai, Junfeng ;
Li, Dan ;
Fang, Xiaona ;
Jiang, Hong ;
Dong, Qingzhe ;
Wang, Erkang .
JOURNAL OF MATERIALS CHEMISTRY, 2010, 20 (41) :9215-9219
[19]   Controlled synthesis, growth mechanism, and properties of monodisperse CdS colloidal spheres [J].
Li, Xin-Hao ;
Li, Ji-Xue ;
Li, Guo-Dong ;
Liu, Da-Peng ;
Chen, Jie-Sheng .
CHEMISTRY-A EUROPEAN JOURNAL, 2007, 13 (31) :8754-8761
[20]   Crystallography of Novel T-Shaped ZnS Nanostructures and Their Cathodoluminescence [J].
Liu, Baodan ;
Bando, Yoshio ;
Wang, Zaien ;
Li, Chengyao ;
Gao, Min ;
Mitome, Masanori ;
Jiang, Xin ;
Golberg, Dmitri .
CRYSTAL GROWTH & DESIGN, 2010, 10 (09) :4143-4147