Glycerol Determination in Biodiesel and Biodiesel Blends According to ASTM D 7591

被引：0
|
作者：
Gandhi, J. [1 ]
Wille, A. [1 ]
机构：
[1] Metrohm, Herisau, Switzerland
来源：
LC GC EUROPE | 2013年
关键词：
D O I：
暂无
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
The presented ion chromatographic (IC) method is applicable to all biodiesel types and blends. Before chromatographic separation, free glycerol and bound glycerol are isolated by a straightforward extraction and saponification-extraction technique. Pulsed amperometric detection (PAD) following chromatographic separation achieves an outstanding method detection limit (MDL) of 0.5 ppm by mass for glycerol and therefore easily fulfills ASTM and EN performance specifications. The described method fully complies with ASTM D 7591.
引用
收藏
页码：10 / 13
页数：4
相关论文
共 50 条
  • [21] Assessment of oxidative stability of biodiesel and biodiesel blends
    Arumugam, Sivashankar
    Muthaiyan, Ravikumar
    Rajendran, Silambarasan
    ENERGY SOURCES PART A-RECOVERY UTILIZATION AND ENVIRONMENTAL EFFECTS, 2023, 45 (02) : 6371 - 6387
  • [22] Engine emissions with biodiesel fuels and biodiesel blends
    May, Bryan W.
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2007, 234
  • [23] Sensing biodiesel and biodiesel-petrodiesel blends
    Kawano, Marianne S.
    Cardoso, Tarik K. M.
    Possetti, Gustavo R. C.
    Kamikawachi, Ricardo C.
    Fabris, Jose L.
    Muller, Marcia
    22ND INTERNATIONAL CONFERENCE ON OPTICAL FIBER SENSORS, PTS 1-3, 2012, 8421
  • [24] A review on prediction of properties of biodiesel and blends of biodiesel
    Saxena, Parag
    Jawale, Sayali
    Joshipura, Milind H.
    CHEMICAL, CIVIL AND MECHANICAL ENGINEERING TRACKS OF 3RD NIRMA UNIVERSITY INTERNATIONAL CONFERENCE ON ENGINEERING (NUICONE2012), 2013, 51 : 395 - 402
  • [25] Comparison of chromatographic methods for the determination of bound glycerol in biodiesel
    Foglia, TA
    Jones, KC
    Nuñez, A
    Phillips, JG
    Mittelbach, M
    CHROMATOGRAPHIA, 2004, 60 (5-6) : 305 - 311
  • [26] Comparison of Chromatographic Methods for the Determination of Bound Glycerol in Biodiesel
    T. A. Foglia
    K. C. Jones
    A. Nuñez
    J. G. Phillips
    M. Mittelbach
    Chromatographia, 2004, 60 : 305 - 311
  • [27] An alternative spectrophotometric method for the determination of free glycerol in biodiesel
    Bondioli, P
    Della Bella, L
    EUROPEAN JOURNAL OF LIPID SCIENCE AND TECHNOLOGY, 2005, 107 (03) : 153 - 157
  • [28] Determination of free and total glycerol in biodiesel by spot analysis
    Carabajal, Maira D.
    Glorio, Alejandra
    Marcipar, Ivan S.
    Lagier, Claudia M.
    MICROCHEMICAL JOURNAL, 2020, 158
  • [29] Catalytic valorization of glycerol for producing biodiesel-compatible biofuel blends
    Al-Mashhadani, Husam A. M.
    Capareda, Sergio C.
    Lacey, Ronald E.
    Fernando, Sandun D.
    BIOFUELS-UK, 2020, 11 (05): : 621 - 635
  • [30] Biodiesel Production from Waste Oil and Its Blends with Glycerol Ketals
    Chipurici, Petre
    Vlaicu, Alexandru
    Raducanu, Cristian Eugen
    Bran, Stefania Daniela
    Gavrila, Adina Ionuta
    REVISTA DE CHIMIE, 2018, 69 (07): : 1881 - 1885
12345