Beyond the ensemble average: X-ray microdiffraction analysis of single SiGe islands

被引:60
作者
Mocuta, C. [1 ]
Stangl, J. [2 ]
Mundboth, K. [1 ,2 ]
Metzger, T. H. [1 ]
Bauer, G. [2 ]
Vartanyants, I. A. [3 ]
Schmidbauer, M. [4 ]
Boeck, T. [4 ]
机构
[1] ESRF, F-38043 Grenoble, France
[2] Johannes Kepler Univ Linz, Inst Halbleiter & Festkorperphys, A-4040 Linz, Austria
[3] Hasylab DESY, D-22607 Hamburg, Germany
[4] Inst Crystal Growth, D-12489 Berlin, Germany
来源
PHYSICAL REVIEW B | 2008年 / 77卷 / 24期
基金
奥地利科学基金会;
关键词
D O I
10.1103/PhysRevB.77.245425
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
X-ray microdiffraction is used to analyze strain and composition profiles in individual micron-sized SiGe islands grown by liquid phase epitaxy on Si(001) substrates. From the variation of the scattered intensity while scanning the sample through a focused x-ray beam of few mu m size, an image of the island distribution on the sample is created. Using this image it is possible to identify particular islands and select them for analysis one by one. The Ge and strain distribution within each island is obtained from the intensity distribution in reciprocal space measured for several individual islands. The detailed shape of each measured island is obtained from scanning electron microscopy. Apart from truncated pyramid-shaped islands, we detect and characterize a small number of flat islands and show that they represent an earlier growth stage of the pyramidal shaped ones. This analysis is only possible by combining the local x-ray diffraction with scanning electron microscopy on exactly the same islands.
引用
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页数:6
相关论文
共 32 条
[1]  
[Anonymous], 2004, X-ray diffuse scattering from self-organized mesoscopic semiconductor structures
[2]   X-ray microdiffraction study of growth modes and crystallographic tilts in oxide films on metal substrates [J].
Budai, JD ;
Yang, WG ;
Tamura, N ;
Chung, JS ;
Tischler, JZ ;
Larson, BC ;
Ice, GE ;
Park, C ;
Norton, DP .
NATURE MATERIALS, 2003, 2 (07) :487-492
[3]   Lattice parameter of Si1-x-yGexCy alloys [J].
De Salvador, D ;
Petrovich, M ;
Berti, M ;
Romanato, F ;
Napolitani, E ;
Drigo, A ;
Stangl, J ;
Zerlauth, S ;
Mühlberger, M ;
Schäffler, F ;
Bauer, G ;
Kelires, PC .
PHYSICAL REVIEW B, 2000, 61 (19) :13005-13013
[4]   Observation of subnanometre-high surface topography with X-ray reflection phase-contrast microscopy [J].
Fenter, Paul ;
Park, Changyong ;
Zhang, Zhan ;
Wang, Steve .
NATURE PHYSICS, 2006, 2 (10) :700-704
[5]   Three-dimensional Si/Ge quantum dot crystals [J].
Gruetzmacher, Detlev ;
Fromherz, Thomas ;
Dais, Christian ;
Stangl, Julian ;
Mueller, Elisabeth ;
Ekinci, Yasin ;
Solak, Harun H. ;
Sigg, Hans ;
Lechner, Rainer T. ;
Wintersberger, Eugen ;
Birner, Stefan ;
Holy, Vaclav ;
Bauer, Guenther .
NANO LETTERS, 2007, 7 (10) :3150-3156
[6]   Critical aspects of alloying and stress relaxation in Ge/Si(100) islands [J].
Hadjisavvas, G ;
Kelires, PC .
PHYSICAL REVIEW B, 2005, 72 (07)
[7]   SiGe/Si(001) Stranski-Krastanow islands by liquid-phase epitaxy:: Diffuse x-ray scattering versus growth observations -: art. no. 075317 [J].
Hanke, M ;
Schmidbauer, M ;
Grigoriev, D ;
Raidt, H ;
Schäfer, P ;
Köhler, R ;
Gerlitzke, AK ;
Wawra, H .
PHYSICAL REVIEW B, 2004, 69 (07)
[8]   Scanning x-ray diffraction with 200 nm spatial resolution [J].
Hanke, M. ;
Dubslaff, M. ;
Schmidbauer, M. ;
Boeck, T. ;
Schoeder, S. ;
Burghammer, M. ;
Riekel, C. ;
Patommel, J. ;
Schroer, C. G. .
APPLIED PHYSICS LETTERS, 2008, 92 (19)
[9]   Effect of overgrowth on shape, composition, and strain of SiGe islands on Si(001) [J].
Hesse, A ;
Stangl, J ;
Holy, V ;
Roch, T ;
Bauer, G ;
Schmidt, OG ;
Denker, U ;
Struth, B .
PHYSICAL REVIEW B, 2002, 66 (08) :853211-853218
[10]   Two-dimensional hard X-ray beam compression by combined focusing and waveguide optics [J].
Jarre, A ;
Fuhse, C ;
Ollinger, C ;
Seeger, J ;
Tucoulou, R ;
Salditt, T .
PHYSICAL REVIEW LETTERS, 2005, 94 (07)