Crystal structure of bis{[4,4,5,5-tetramethyl-2-(1-methyl-1H-benzimidazol-2-yl)-4,5-dihydroimidazole-1-oxyl-3-oxide-κ2N,O]-(μ2-thiocyanato-N:S)(thiocyanato-κS)mercury(II)}, Hg2(C15H19N4O2)2(SCN)4

被引：0
作者：
Lou, Shu-Fang [1 ]
Wang, Qing [1 ]
Ding, Jie [1 ]
机构：
[1] Shangqiu Med Coll, Common Subjects Dept, Shangqiu 476100, Peoples R China
来源：
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2012年 / 227卷 / 02期
关键词：
NITRONYL NITROXIDES; MAGNETIC-PROPERTIES; FREE-RADICALS; BIRADICALS; COMPLEXES;
D O I：
10.1524/ncrs.2012.0048
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
C34H38Hg2N12O4S4, triclinic, P (1) over bar (no. 2), a = 7.0767(5) angstrom, b = 12.0722(8) angstrom, c = 12.6814(8) angstrom, alpha = 81.813(1)degrees, beta = 89.790(1)degrees, gamma = 76.450(1)degrees, V = 1042.0 angstrom(3), z = 1, R-gt(F) = 0.020, wR(ref)(F-2) = 0.051, T = 291 K.
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页码：105 / 106
页数：2
相关论文
共 9 条
  • [1] MAGNETIC COUPLING IN ZERO-DIMENSIONAL AND ONE-DIMENSIONAL MAGNETIC SYSTEMS FORMED BY NICKEL(II) AND NITRONYL NITROXIDES - MAGNETIC PHASE-TRANSITION OF A FERRIMAGNETIC CHAIN
    CANESCHI, A
    GATTESCHI, D
    RENARD, JP
    REY, P
    SESSOLI, R
    [J]. INORGANIC CHEMISTRY, 1989, 28 (15) : 2940 - 2944
  • [2] Approach to a single-component ferrimagnetism by organic radical crystals
    Hosokoshi, Y
    Katoh, K
    Nakazawa, Y
    Nakano, H
    Inoue, K
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2001, 123 (32) : 7921 - 7922
  • [3] Kahn O., 1993, MOL MAGNETISM
  • [4] Crystal structures and magnetic properties of mercury(II) bromide complexes with pyridyl-substituted N-oxyl N′-oxides (nitronyl nitroxides)
    Lee, CJ
    Huang, CH
    Wei, HH
    Liu, YH
    Lee, GH
    Wang, Y
    [J]. JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1998, (01): : 171 - 176
  • [5] STUDIES OF FREE RADICALS .I. ALPHA-NITRONYL NITROXIDES A NEW CLASS OF STABLE RADICALS
    OSIECKI, JH
    ULLMAN, EF
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1968, 90 (04) : 1078 - &
  • [6] A short history of SHELX
    Sheldrick, George M.
    [J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122
  • [7] 2D and 3D Cu(hfac)2 complexes with nitronyl nitroxide biradicals
    Tretyakov, E
    Fokin, S
    Romanenko, G
    Ikorskii, V
    Vasilevsky, S
    Ovcharenko, V
    [J]. INORGANIC CHEMISTRY, 2006, 45 (09) : 3671 - 3678
  • [8] STUDIES OF STABLE FREE RADICALS .20. NITRONYL NITROXIDE MONORADICALS AND BIRADICALS AS POSSIBLE SMALL MOLECULE SPIN LABELS
    ULLMAN, EF
    OSIECKI, JH
    BOOCOCK, DGB
    DARCY, R
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1972, 94 (20) : 7049 - +
  • [9] Synthesis, structure and magnetic properties of a novel lead(II) complex containing nitronyl nitroxide radicals
    Wang, Li-Ya
    Wang, Yu-Fang
    Ma, Lu-Fang
    [J]. INORGANIC CHEMISTRY COMMUNICATIONS, 2007, 10 (12) : 1444 - 1447
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