N′-[(E)-1-phenylethylidene]benzohydrazide

被引:17
作者
Fun, Hoong-Kun [1 ]
Sujith, K. V. [2 ]
Patil, P. S. [3 ]
Kalluraya, B. [2 ]
Chantrapromma, Suchada [4 ]
机构
[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, George Town 11800, Malaysia
[2] Mangalore Univ, Dept Studies Chem, Mangalagangothri 574199, Karnataka, India
[3] KLE Inst Technol, KLE Soc, Dept Phys, Hubli 590030, India
[4] Prince Songkla Univ, Fac Sci, Dept Chem, Crystal Mat Res Unit, Hat Yai 90112, Songkhla, Thailand
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷
关键词
D O I
10.1107/S1600536808029218
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C15H14N2O, crystallized with two independent molecules in the asymmetric unit. Both molecules are non-planar and have an E configuration with respect to the C N bond. The dihedral angles between the two benzene rings are 11.1 (2)degrees in one molecule and 12.40 (19)degrees in the other. In the crystal structure, the molecules are linked by N-H center dot center dot center dot O hydrogen bonds and weak C-H center dot center dot center dot O interactions into infinite one-dimensional chains along [1 0 0]. The crystal structure is further stabilized by N-H center dot center dot center dot O hydrogen bonds, weak C-H center dot center dot center dot O and very weak C-H center dot center dot center dot pi interactions.
引用
收藏
页码:O1961 / U4094
页数:13
相关论文
共 9 条
[1]   TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS [J].
ALLEN, FH ;
KENNARD, O ;
WATSON, DG ;
BRAMMER, L ;
ORPEN, AG ;
TAYLOR, R .
JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12) :S1-S19
[2]  
Bratenko M. K., 1999, CHEM HETEROCYCL COMP, V35, P1075
[3]  
Bruker, 2005, APEX2 SAINT SADABS
[4]   Synthesis of some bioactive 2-bromo-5-methoxy-N′-[4-(aryl)-1,3-thiazol-2-yl]benzohydrazide derivatives [J].
Raj, K. K. Vijaya ;
Narayana, B. ;
Ashalatha, B. V. ;
Kumari, N. Suchetha ;
Sarojini, B. K. .
EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2007, 42 (03) :425-429
[5]   Synthesis and antimicrobial activity of some new hydrazones of 4-fluorobenzoic acid hydrazide and 3-acetyl-2,5-disubstituted-1,3,4-oxadiazolines [J].
Rollas, S ;
Gulerman, N ;
Erdeniz, H .
FARMACO, 2002, 57 (02) :171-174
[6]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[7]   Single-crystal structure validation with the program PLATON [J].
Spek, AL .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 :7-13
[8]   Synthesis of novel 1-H-pyrazole-4-carboxylic acid esters by conventional and microwave assisted Vilsmeier cyclization of hydrazones [J].
Sridhar, R ;
Perumal, PT .
SYNTHETIC COMMUNICATIONS, 2003, 33 (09) :1483-1488
[9]  
ZHANG X, 2007, BIOORG MED CHEM LETT, V17, P3774