Synthesis and crystal structure of 5-(8(((2-carboxyethyl)ammonio) methyl)-7-hydroxy-4-oxo-4H-chromen-3-yl)-2-hydroxybenzenesulfonate trihydrate, C19H23NO12S

被引：2
作者：
Chen, Hai-Lin [1 ]
Yin, Xiu-Ju [1 ]
机构：
[1] Hechi Univ, Coll Chem & Biol Engn, Hechi 547000, Peoples R China
来源：
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2019年 / 234卷 / 02期
关键词：
SODIUM; ISOFLAVONOIDS; SULFONATE; ANALOGS;
D O I：
10.1515/ncrs-2018-0307
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
C19H23NO12S, triclinic, P (1) over bar (no. 2), a = 8.3926(9) angstrom, b = 9.0469(6) angstrom, c = 15.3442(15) angstrom, alpha = 78.195(7)degrees, beta= 74.352(9)degrees, gamma = 70.169(8)degrees, V = 1047.08(18) angstrom(3), Z = 2, R-gt (F) = 0.0538, WRref(F-2) = 0.1289, T = 293(2) K.
引用
收藏
页码：265 / 267
页数：3
相关论文
共 17 条
  • [1] Aitmambetov A., 1994, CHEM NAT COMPD, V30, P576
  • [2] Bruker: A., 2016, APEX3 SAINT PLUS XPR
  • [3] Chen H.-L., 2018, NCS, V233, P469
  • [4] Synthesis and crystal structure of trans-tetraqua-bis(2-(((7-hydroxy-3-(4-hydroxy-3-sulfonatophenyl)-4-oxo-4H-chromen-8-yl)methyl) ammonio)acetato-κO)cobalt(II) hexahydrate, C36H48CoN2O28S2
    Chen, Hai-Lin
    Lai, Hong-Fang
    Wei, Lian-Qiang
    Jiang, Li-Rong
    Su, Yan-Xiang
    [J]. ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2017, 232 (06): : 1025 - 1027
  • [5] Chen HL, 2014, Z KRIST-NEW CRYST ST, V229, P476, DOI [10.1515/ncrs-2014-0127, 10.1515/ners-2014-0127]
  • [6] Synthesis of analogs of natural 2′-methoxyisoflavones
    Frasinyuk, M. S.
    Bondarenko, S. P.
    Khilya, V. P.
    [J]. CHEMISTRY OF NATURAL COMPOUNDS, 2006, 42 (02) : 142 - 147
  • [7] Synthesis of amino-acid derivatives of formononetin and cladrin
    Frasinyuk, M. S.
    Mrug, G. P.
    Fedoryak, O. D.
    Bondarenko, S. P.
    [J]. CHEMISTRY OF NATURAL COMPOUNDS, 2012, 48 (04) : 570 - 573
  • [8] Antineoplastic Isoflavonoids Derived from Intermediate ortho-Quinone Methides Generated from Mannich Bases
    Frasinyuk, Mykhaylo S.
    Mrug, Galyna P.
    Bondarenko, Svitlana P.
    Khilya, Volodymyr P.
    Sviripa, Vitaliy M.
    Syrotchuk, Oleksandr A.
    Zhang, Wen
    Cai, Xianfeng
    Fiandalo, Michael V.
    Mohler, James L.
    Liu, Chunming
    Watt, David S.
    [J]. CHEMMEDCHEM, 2016, 11 (06) : 600 - 611
  • [9] Application of Mannich bases to the synthesis of hydroxymethylated isoflavonoids as potential antineoplastic agents
    Frasinyuk, Mykhaylo S.
    Mrug, Galyna P.
    Bondarenko, Svitlana P.
    Sviripa, Vitaliy M.
    Zhang, Wen
    Cai, Xianfeng
    Fiandalo, Michael V.
    Mohler, James L.
    Liu, Chunming
    Watt, David S.
    [J]. ORGANIC & BIOMOLECULAR CHEMISTRY, 2015, 13 (46) : 11292 - 11301
  • [10] Huang, 2018, NCS, V233, P417
12