Empirical Modeling of Nano Alumina Combustion Synthesis Using Box-Behnken Statistical Design

被引：3

作者：

Edrissi, Mohammad ^{[1
]}

Norouzbeigi, Reza ^{[2
]}

机构：

[1] Amirkabir Univ Technol, Chem Engn Fac, Tehran, Iran

[2] Iran Univ Sci & Technol, Sch Chem Engn, Tehran, Iran

来源：

SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2014年 / 44卷 / 06期

关键词：

modeling; electron microscopy; alumina; combustion synthesis; OIL-SHALE ASH; GAMMA-ALUMINA; POWDERS; SURFACE; OPTIMIZATION; GEL; PRECIPITATION; TEMPERATURE; HYDROLYSIS; RATIO;

D O I：

10.1080/15533174.2013.791838

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Nano-sized Al2O3 has been prepared by combustion synthesis. The process has been empirically modeled using Box-Behnken design method for the first time. The products were characterized by XRD, BET, TGA, FESEM, and TEM analyses. Results demonstrated that the nano alumina powders had specific surface areas between 37m(2)/g and 113m(2)/g. The synthesis of alumina was modified in order to achieve higher specific surface area (154m(2)/g). This method has been resulted nano fibers with the length and diameter of about 150 and 10nm, respectively.

引用

页码：804 / 813

页数：10

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