Empirical Modeling of Nano Alumina Combustion Synthesis Using Box-Behnken Statistical Design

被引:3
作者
Edrissi, Mohammad [1 ]
Norouzbeigi, Reza [2 ]
机构
[1] Amirkabir Univ Technol, Chem Engn Fac, Tehran, Iran
[2] Iran Univ Sci & Technol, Sch Chem Engn, Tehran, Iran
关键词
modeling; electron microscopy; alumina; combustion synthesis; OIL-SHALE ASH; GAMMA-ALUMINA; POWDERS; SURFACE; OPTIMIZATION; GEL; PRECIPITATION; TEMPERATURE; HYDROLYSIS; RATIO;
D O I
10.1080/15533174.2013.791838
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Nano-sized Al2O3 has been prepared by combustion synthesis. The process has been empirically modeled using Box-Behnken design method for the first time. The products were characterized by XRD, BET, TGA, FESEM, and TEM analyses. Results demonstrated that the nano alumina powders had specific surface areas between 37m(2)/g and 113m(2)/g. The synthesis of alumina was modified in order to achieve higher specific surface area (154m(2)/g). This method has been resulted nano fibers with the length and diameter of about 150 and 10nm, respectively.
引用
收藏
页码:804 / 813
页数:10
相关论文
共 61 条
  • [1] Thermal behaviour of alumina precursor obtained by the aluminium sulphate-urea reaction in boiling aqueous solution
    Ada, K
    Sarikaya, Y
    Alemdaroglu, T
    Önal, M
    [J]. CERAMICS INTERNATIONAL, 2003, 29 (05) : 513 - 518
  • [2] [Anonymous], 2007, MODERN EXPT DESIGN
  • [3] Aruna A. S., 2004, MAT RES B, V39, P157
  • [4] Combustion synthesis and nanomaterials
    Aruna, Singanahally T.
    Mukasyan, Alexander S.
    [J]. CURRENT OPINION IN SOLID STATE & MATERIALS SCIENCE, 2008, 12 (3-4) : 44 - 50
  • [5] A Box-Behnken design for determining the optimum experimental condition of the fungicide (Vapam) sorption onto soil modified with perlite
    Azizi, Seyed N.
    Asemi, Neda
    [J]. JOURNAL OF ENVIRONMENTAL SCIENCE AND HEALTH PART B-PESTICIDES FOOD CONTAMINANTS AND AGRICULTURAL WASTES, 2012, 47 (07) : 692 - 699
  • [6] Effect of citrate to nitrate ratio on the decomposition characteristics and phase formation of alumina
    Banerjee, S.
    Devi, P. Sujatha
    [J]. JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 2007, 90 (03) : 699 - 706
  • [7] Auto ignition processing of nanocrystalline alpha-Al2O3
    Bhaduri, S
    Zhou, E
    Bhaduri, SB
    [J]. NANOSTRUCTURED MATERIALS, 1996, 7 (05): : 487 - 496
  • [8] Alumina-zirconia-yttria nanocomposites prepared by solution combustion synthesis
    Biamino, S.
    Fino, P.
    Pavese, M.
    Badini, C.
    [J]. CERAMICS INTERNATIONAL, 2006, 32 (05) : 509 - 513
  • [9] Influence of combustion aids on suspension combustion synthesis of mullite powders
    Burgos-Montes, O.
    Moreno, R.
    Colomer, M. T.
    Farinas, J. C.
    [J]. JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2006, 26 (15) : 3365 - 3372
  • [10] Influence of citric acid to aluminium nitrate molar ratio on the combustion synthesis of alumina-zirconia nanopowders
    Chandradass, J.
    Kim, Myong Ho
    Bae, Dong-Sik
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2009, 470 (1-2) : L9 - L12