Vortex grinding for mechanochemistry: application for automated supramolecular catalysis and preparation of a metal-organic framework

被引：72
作者：
Stojakovic, Jelena [1 ]
Farris, Brian S. [1 ]
MacGillivray, Leonard R. [1 ]
机构：
[1] Univ Iowa, Dept Chem, Iowa City, IA 52242 USA
来源：
CHEMICAL COMMUNICATIONS | 2012年 / 48卷 / 64期
基金：
美国国家科学基金会;
关键词：
SOLID-STATE; REACTIVITY; NANOPARTICLES; KINETICS; BASICS; C-60;
D O I：
10.1039/c2cc33227b
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
An automated grinding method based on a vortex mixer has been developed. The method enables simultaneous grinding and UV-irradiation, as well as in situ monitoring of solid-state reactivity. The method has been applied to a cocrystallization, supramolecular catalysis, and the preparation of a metal-organic framework.
引用
收藏
页码：7958 / 7960
页数：3
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