Vortex grinding for mechanochemistry: application for automated supramolecular catalysis and preparation of a metal-organic framework

被引：72

作者：

Stojakovic, Jelena ^{[1
]}

Farris, Brian S. ^{[1
]}

MacGillivray, Leonard R. ^{[1
]}

机构：

[1] Univ Iowa, Dept Chem, Iowa City, IA 52242 USA

来源：

CHEMICAL COMMUNICATIONS | 2012年 / 48卷 / 64期

基金：

美国国家科学基金会;

关键词：

SOLID-STATE; REACTIVITY; NANOPARTICLES; KINETICS; BASICS; C-60;

D O I：

10.1039/c2cc33227b

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An automated grinding method based on a vortex mixer has been developed. The method enables simultaneous grinding and UV-irradiation, as well as in situ monitoring of solid-state reactivity. The method has been applied to a cocrystallization, supramolecular catalysis, and the preparation of a metal-organic framework.

引用

收藏

页码：7958 / 7960

页数：3

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