Exploratory syntheses, crystal structures, and properties of two new 3-D coordination polymers of Mn(II) and Fe(II) with (54.62) (510.63.7.8) topological spaces

被引：17

作者：

Fan, Liming ^{[1
,2
]}

Zhang, Xiutang ^{[1
,2
]}

Sun, Zhong ^{[2
]}

Zhang, Wei ^{[2
]}

Li, Dacheng ^{[1
]}

Wei, Peihai ^{[2
]}

Li, Bin ^{[2
]}

Dou, Jianmin ^{[1
]}

机构：

[1] Liaocheng Univ, Coll Chem & Chem Engn, Liaocheng 252059, Peoples R China

[2] Qilu Normal Univ, Adv Mat Inst Res, Dept Chem & Chem Engn, Jinan 250013, Peoples R China

来源：

JOURNAL OF COORDINATION CHEMISTRY | 2012年 / 65卷 / 24期

关键词：

terphenyl-2; 5; 2'; 5'-tetracarboxylic acid; 1; 2-bis(diphenylphosphoryl)ethane; manganese(II); iron(II); METAL-ORGANIC FRAMEWORKS; CO-LIGANDS; COMPLEXES; ACID; ARCHITECTURES; CLUSTERS; TECTON; SERIES;

D O I：

10.1080/00958972.2012.741684

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Solvothermal reactions of terphenyl-2,5,2',5'-tetracarboxylic acid (H4qptc) and MII (M = Mn, Fe) in the presence of 1,2-bis(diphenylphosphino)ethane (dppe) afford two new coordination polymers, [M(qptc)(dppe-O)] n (M?=?Mn (1), Fe (2)) (1,2-bis(diphenylphosphoryl)ethane?=?dppe-O). The structures have been determined by single-crystal X-ray diffraction analyses and further characterized by elemental analyses, IR, TGA, and magnetism. The MII in 1 and 2 are linked by qptc4- to form 2-D layers, which are further connected via the oxidized dppe (dppe-O) exhibiting a (4,6)-connected network with the (54.62)(510.63.7.8) topology.

引用

页码：4389 / 4396

页数：8

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