Effect of pressure on crystalline L- and DL-serine: revisited by a combined single-crystal X-ray diffraction at a laboratory source and polarized Raman spectroscopy study

被引：31
|
作者：
Zakharov, Boris A. [1 ,2 ]
Kolesov, Boris A. [2 ,3 ]
Boldyreva, Elena V. [1 ,2 ]
机构：
[1] Inst Solid State Chem & Mechochem SB RAS, Novosibirsk, Russia
[2] REC 008 Novosibirsk State Univ, Novosibirsk, Russia
[3] Inst Inorgan Chem SB RAS, Novosibirsk, Russia
来源：
ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE CRYSTAL ENGINEERING AND MATERIALS | 2012年 / 68卷
关键词：
INDUCED PHASE-TRANSITIONS; ABSORPTION CORRECTIONS; INCREASING PRESSURE; NEUTRON-DIFFRACTION; HYDROGEN-BONDS; AMINO-ACIDS; L-ALANINE; 100; K; POLYMORPH; GLYCINE;
D O I：
10.1107/S0108768112015960
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Information on the effect of pressure on hydrogen bonds, which could be derived from single-crystal X-ray diffraction at a laboratory source and polarized Raman spectroscopy, has been compared. l-Serine and DL-serine were selected for this case study. The role of hydrogen bonds in pressure-induced phase transitions in the first system and in the structural stability of the second one are discussed. Non-monotonic distortion of selected hydrogen bonds in the pressure range below similar to 1-2 GPa, a change in the compression mechanism at similar to 2-3 GPa, and the evidence of formation of bifurcated N-H center dot center dot center dot O hydrogen bonds in DL-serine at similar to 3-4 GPa are considered.
引用
收藏
页码：275 / 286
页数：12
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