Crystal structure of (Z)-N′-[amino(pyridin-2-yl)-methylene]-2-hydroxybenzohydrazide, C13H12N4O2

被引:4
作者
Zhu, Guang-Zhou [1 ]
Lu, Zai-Sheng [1 ]
Shi, Huan-Le [2 ]
Xu, Suo-Ping [1 ]
Lu, Huan [1 ]
Wang, Xiang-Shan [1 ]
机构
[1] Jiangsu Normal Univ, Sch Chem & Chem Engn, Jiangsu Key Lab Green Synthet Chem Funct Mat, Xuzhou 221116, Jiangsu, Peoples R China
[2] Lianyungang Henrychem Sci Co Let, Lianyungang 222000, Jiangsu, Peoples R China
来源
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES | 2012年 / 227卷 / 04期
基金
中国国家自然科学基金;
关键词
D O I
10.1524/ncrs.2012.0263
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
C13H12N4O2, monoclinic, Cc (no. 9), a = 8.749(4) angstrom, b = 17.707(8) angstrom, c = 8.005(4) angstrom, beta = 102.751(5)degrees, V = 1209.5 angstrom(3), Z = 4, R-gt(F) = 0.0270, wR(ref)(F-2) = 0.0701, T = 296 K.
引用
收藏
页码:533 / 534
页数:2
相关论文
共 5 条
[1]  
Browne E.J., 1968, J CHEM SOC C, V7, P824
[2]   Bis[N3-(2-hydroxybenzoyl)pyridine-2-carboxamidrazonato-κ3N1,N2,O]zinc(II) [J].
Li, Yong .
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 :M2837-U1924
[3]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[4]   THE 1ST DINUCLEAR MU-HEXAFLUOROSILICATO COPPER(II) COMPOUND - SYNTHESIS AND CRYSTAL-STRUCTURE OF (MU-HEXAFLUOROSILICATO-KAPPA-F-KAPPA-F')-BIS[AQUA(N3-SALICYLOYLPYRIDINE-2-CARBOXAMIDRAZONATO-KAPPA(3)N',N2,O)COPPER(II)] DIHYDRATE [J].
VANKONINGSBRUGGEN, PJ ;
HAASNOOT, JG ;
DEGRAAFF, RAG ;
REEDIJK, J .
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1993, (03) :483-484
[5]   SYNTHESES, SPECTROSCOPIC AND MAGNETIC-PROPERTIES AND X-RAY CRYSTAL-STRUCTURE OF 2 DINUCLEAR COPPER(II) COMPOUNDS WITH THE LIGAND N-3-SALICYLOYLPYRIDINE-2-CARBOXAMIDRAZONATO [J].
VANKONINGSBRUGGEN, PJ ;
HAASNOOT, JG ;
DEGRAAFF, RAG ;
REEDIJK, J .
INORGANICA CHIMICA ACTA, 1995, 234 (1-2) :87-94