Analysis of Volatile Oil of Fritillaria cirrhosa D. Don by GC-MS

被引:2
作者
Wang, Xiaojing [1 ]
Li, Yumei [2 ]
机构
[1] Tianjin Univ, Sch Chem Engn & Technol, Tianjin 300072, Peoples R China
[2] Dezhou Univ, Dept Chem, Shandong 253023, Peoples R China
关键词
Fritillaria cirrhosa D. Don; Volatile oil; Water steam distillation; Gas chromatography-mass spectrometry; ISOSTEROIDAL ALKALOIDS; STEROIDAL ALKALOIDS; BULBS;
D O I
10.14233/ajchem.2013.13617
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The volatile oil was extracted from Fritillaria cirrhosa D. Don by water steam distillation and the chemical constituents of volatile oil separated were identified by gas chromatography-mass spectrometry analysis. The relative content of the constituents from the volatile oil were determined by area normalization method. Thirty-nine peaks were separated, among which 14 compounds were identified, amounting to 81.92 % of the total amount of volatile oil. The main compounds identified to be 1-octadecene (16.38 %), 1-dodecene (15.09), oxirane, hexadecyl-(11.38 %), 1-hexadecanol (10.65 %), 1-eicosanol (7.95 %), 9-octadecynoic acid, methyl ester (6.94 %), n-hexadecanoic acid (5.41 %). The work provides information for making full use of the Fritillaria cirrhosa D. Don resources and pharmacological activities research of traditional Chinese medicine.
引用
收藏
页码:3252 / 3254
页数:3
相关论文
共 9 条
[1]   Steroidal alkaloids from the bulbs of Fritillaria puqiensis [J].
Jiang, Y ;
Li, HJ ;
Li, P ;
Cai, ZH ;
Ye, WC .
JOURNAL OF NATURAL PRODUCTS, 2005, 68 (02) :264-267
[2]   Phytochemical Variation in Fritillaria cirrhosa D. Don (Chuan Bei Mu) in Relation to Plant Reproductive Stage and Timing of Harvest [J].
Konchar, Katie ;
Li, Xiao-Li ;
Yang, Yong-Ping ;
Emshwiller, Eve .
ECONOMIC BOTANY, 2011, 65 (03) :283-294
[3]   Chemistry, bioactivity and geographical diversity of steroidal alkaloids from the Liliaceae family [J].
Li, Hui-Jun ;
Jiang, Yan ;
Li, Ping .
NATURAL PRODUCT REPORTS, 2006, 23 (05) :735-752
[4]   Determination of the major isosteroidal alkaloids in bulbs of Fritillaria by high-performance liquid chromatography coupled with evaporative light scattering detection [J].
Li, SL ;
Lin, G ;
Chan, SW ;
Li, P .
JOURNAL OF CHROMATOGRAPHY A, 2001, 909 (02) :207-214
[5]   Selective antagonism activity of alkaloids from bulbs Fritillariae at muscarinic receptors:: Functional studies [J].
Lin, Bao-Qin ;
Ji, Hui ;
Li, Ping ;
Jiang, Yan ;
Fang, Wei .
EUROPEAN JOURNAL OF PHARMACOLOGY, 2006, 551 (1-3) :125-130
[6]   Inhibitors of acetylcholine esterase in vitro screening of steroidal alkaloids from Fritillaria species [J].
Lin, Bao-Qin ;
Ji, Hui ;
Li, Ping ;
Fang, Wei ;
Jiang, Yan .
PLANTA MEDICA, 2006, 72 (09) :814-818
[7]   Chromatographic analysis of Fritillaria isosteroidal alkaloids, the active ingredients of Beimu, the antitussive traditional Chinese medicinal herb [J].
Lin, G ;
Li, P ;
Li, SL ;
Chan, SW .
JOURNAL OF CHROMATOGRAPHY A, 2001, 935 (1-2) :321-338
[8]  
Pharmacopoeia Committee of Chinese Ministry of Health, 2005, PHARM PEOPL REP CHIN, V25
[9]   Structural elucidation of fritillahupehin from bulbs of Fritillaria hupehensis Hsiao et KC Hsia [J].
Zhang, YH ;
Ruan, HL ;
Pi, HF ;
Wu, JZ ;
Sun, HD ;
Fujita, T .
JOURNAL OF ASIAN NATURAL PRODUCTS RESEARCH, 2004, 6 (01) :29-34