Differentiation of Turkish Rakies through Headspace Solid-Phase Microextraction and Gas Chromatography-Mass Spectrometry Analysis

被引：5

作者：

Yilmaztekin, M. ^{[1
]}

Cabaroglu, T. ^{[2
]}

Gunata, Z. ^{[3
]}

机构：

[1] Inonu Univ, Dept Food Engn, Fac Engn, TR-44280 Malatya, Turkey

[2] Cukurova Univ, Dept Food Engn, Fac Agr, TR-01330 Adana, Turkey

[3] Univ Montpellier 2, UMR Qualisud, F-34095 Montpellier 5, France

来源：

JOURNAL OF THE INSTITUTE OF BREWING | 2011年 / 117卷 / 04期

关键词：

anethole; estragole; gas chromatography-mass spectrometry; PCA; solid-phase microextraction; Turkish raki; METHANOL; AROMA;

D O I：

10.1002/j.2050-0416.2011.tb00513.x

中图分类号：

TS2 [食品工业];

学科分类号：

0832 ;

摘要：

J. Inst. Brew. 117(4), 622-626, 2011 Composition of flavour compounds from several commercial raki samples was determined through headspace solid-phase microextraction (HS-SPME) and gas chromatography coupled to mass spectrometry (GC MS). The extraction of volatile compounds was performed using a 75 mu m CAR/PDMS fibre. Forty three volatile compounds were identified. The major compounds were trans-anethole (86.47-94.19%), valencene (1.15-6.77%), estragole (2.66-5.46%), and cis-anethole (0.72-2.33%). Principal component analysis (PCA) enabled the differentiation of the raki samples thanks to compounds arising mainly from aniseed.

引用

页码：622 / 626

页数：5

共 13 条

[1] Methanol and Major Volatile Compounds of Turkish Raki and Effect of Distillate Source [J].

Cabaroglu, Turgut ;

Yilmaztekin, Murat .

JOURNAL OF THE INSTITUTE OF BREWING, 2011, 117 (01) :98-105

[2] Comparative study of the whisky aroma profile based on headspace solid phase microextraction using different fibre coatings [J].

Camara, J. S. ;

Marques, J. C. ;

Perestrelo, R. M. ;

Rodrigues, F. ;

Oliveira, L. ;

Andrade, P. ;

Caldeira, M. .

JOURNAL OF CHROMATOGRAPHY A, 2007, 1150 (1-2) :198-207

[3]

Ebeler SE, 2000, J SCI FOOD AGR, V80, P625, DOI 10.1002/(SICI)1097-0010(200004)80:5<625::AID-JSFA584>3.3.CO

[4]

2-X

[5] Characterisation of whiskeys using solid-phase microextraction with gas chromatography-mass spectrometry [J].

Fitzgerald, G ;

James, KJ ;

MacNamara, K ;

Stack, MA .

JOURNAL OF CHROMATOGRAPHY A, 2000, 896 (1-2) :351-359

[6] Characterization of aniseed-flavoured spirit drinks by headspace solid-phase microextraction gas chromatography-mass spectrometry and chemometrics [J].

Jurado, J. M. ;

Ballesteros, O. ;

Alcazar, A. ;

Pablos, F. ;

Martin, M. J. ;

Vilchez, J. L. ;

Navalon, A. .

TALANTA, 2007, 72 (02) :506-511

[7] Volatiles in distillates of cider aged in American oak wood [J].

Mangas, J ;

Rodriguez, R ;

Moreno, J ;

Blanco, D .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1996, 44 (01) :268-273

[8] Monoterpenes in grape juice and wines [J].

Mateo, JJ ;

Jiménez, M .

JOURNAL OF CHROMATOGRAPHY A, 2000, 881 (1-2) :557-567

[9]

Ng L.-K., 1999, Applications of Solid Phase Microextraction, P393, DOI [10.1039/9781847550149-00393, DOI 10.1039/9781847550149-00393]

[10] Gas chromatographic-mass spectrometric analysis of essential oils from Pimpinella species gathered from Central and Northern Turkey [J].

Tabanca, N ;

Demirci, B ;

Ozek, T ;

Kirimer, N ;

Baser, KHC ;

Bedir, E ;

Khan, IA ;

Wedge, DE .

JOURNAL OF CHROMATOGRAPHY A, 2006, 1117 (02) :194-205

← 1 2 →