Synthesis and Structure of Triphenylbismuth Bis(3-phenylprop-2-enoate)

被引：4
作者：
Andreev, P. V. [1 ]
Somov, N. V. [1 ]
Kalistratova, O. S. [1 ]
Gushchin, A. V. [1 ]
Chuprunov, E. V. [1 ]
机构：
[1] Lobachevsky State Univ Nizhny Novgorod, Nizhnii Novgorod 603950, Russia
来源：
CRYSTALLOGRAPHY REPORTS | 2015年 / 60卷 / 04期
基金：
俄罗斯基础研究基金会;
关键词：
Crystallography Report; Cinnamic Acid; Cinnamate; Bismuth Atom; Triphenylantimony;
D O I：
10.1134/S1063774515040057
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The newly synthesized triphenylbismuth bis(3-phenylprop-2-enoate) was studied by X-ray diffraction and by IR, UV, and NMR spectroscopy. The crystals are monoclinic, sp. gr. C2/c, Z = 4, a = 13.2820(4) angstrom, b = 21.3750(2) angstrom, c = 12.2407(2) angstrom, beta = 119.936(1)degrees. The coordination polyhedron of the bismuth atom can be described as a distorted pentagonal bipyramid.
引用
收藏
页码：517 / 520
页数：4
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