Thermal, structural and rheological behaviour of native and modified waxy corn starch with hydrochloric acid at different temperatures

被引:44
|
作者
de Oliveira, Cristina Soltovski [1 ]
Pereira Andrade, Marina Morena [1 ]
Denck Colman, Tiago Andre [1 ]
Oliveira Gomes da Costa, Fernanda Janaina [2 ]
Schnitzler, Egon [1 ]
机构
[1] UEPG Ponta Grossa State Univ, BR-84030900 Ponta Grossa, PR, Brazil
[2] UFPR Fed Univ Parana, BR-81531980 Curitiba, PR, Brazil
关键词
Waxy corn starch; Acid-modified starch; Atomic force microscopy; Thermal analysis; PHYSICOCHEMICAL PROPERTIES; HIGH-AMYLOSE; MAIZE; GRANULES;
D O I
10.1007/s10973-013-3307-9
中图分类号
O414.1 [热力学];
学科分类号
摘要
In this study, samples of native waxy corn starch, waxy corn starch treated with HCl 0.15 mol L-1 at 20 and 50 A degrees C, respectively, were analysed. The thermogravimetric curves showed similar behaviour with three main mass losses and a decrease in the thermal stability. The acid hydrolysis in low HCl concentration performed for 4 h caused a decrease in peak temperature (DSC), viscosity peak (RVA), gelatinisation enthalpy (DSC) and relative crystallinity (XRD), and an increase in the average roughness (NC-AFM). The X-ray diffraction patterns displayed the 'A' type for all the starch granules.
引用
收藏
页码:13 / 18
页数:6
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