Surface Roughness and Morphology Customization of Additive Manufactured Open Porous Ti6Al4V Structures

被引:196
作者
Pyka, Grzegorz [1 ,2 ]
Kerckhofs, Greet [1 ,2 ,3 ]
Papantoniou, Ioannis [2 ,4 ]
Speirs, Mathew [5 ]
Schrooten, Jan [1 ,2 ]
Wevers, Martine [1 ]
机构
[1] Katholieke Univ Leuven, Dept Met & Mat Engn, B-3001 Louvain, Belgium
[2] Katholieke Univ Leuven, Div Skeletal Tissue Engn, Prometheus, B-3001 Louvain, Belgium
[3] Univ Liege, Biomech Res Unit, B-4000 Liege, Belgium
[4] Katholieke Univ Leuven, Skeletal Biol & Engn Res Ctr, Lab Tissue Engn, Prometheus, B-3001 Louvain, Belgium
[5] Katholieke Univ Leuven, Dept Mech Engn, Div Prod Engn Machine Design & Automat, B-3001 Louvain, Belgium
基金
欧洲研究理事会;
关键词
Ti6Al4V scaffolds; selective laser melting; surface roughness; surface modification; biomaterials; LASER; MICROSTRUCTURE; OPTIMIZATION; PARAMETERS; TITANIUM; CELLS; SAMPLES; DESIGN;
D O I
10.3390/ma6104737
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Additive manufacturing (AM) is a production method that enables the building of porous structures with a controlled geometry. However, there is a limited control over the final surface of the product. Hence, complementary surface engineering strategies are needed. In this work, design of experiments (DoE) was used to customize post AM surface treatment for 3D selective laser melted Ti6Al4V open porous structures for bone tissue engineering. A two-level three-factor full factorial design was employed to assess the individual and interactive effects of the surface treatment duration and the concentration of the chemical etching solution on the final surface roughness and beam thickness of the treated porous structures. It was observed that the concentration of the surface treatment solution was the most important factor influencing roughness reduction. The designed beam thickness decreased the effectiveness of the surface treatment. In this case study, the optimized processing conditions for AM production and the post-AM surface treatment were defined based on the DoE output and were validated experimentally. This allowed the production of customized 3D porous structures with controlled surface roughness and overall morphological properties, which can assist in more controlled evaluation of the effect of surface roughness on various functional properties.
引用
收藏
页码:4737 / 4757
页数:21
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