Analysis of the volatiles generated during the Selby-Noack test by 31P NMR spectroscopy

被引：0
|
作者：
Bosch, RJ [1 ]
Fee, DC [1 ]
Selby, TW [1 ]
机构：
[1] Astaris LLC, Webster Groves, MO 63119 USA
来源：
Elemental Analysis of Fuels and Lubricants: Recent Advances and Future Prospects | 2005年 / 1468卷
关键词：
phosphorus volatility; exhaust catalyst; exhaust emissions; ZDDP; zinc dithiophosphates; phosphorus emission index; PEI; P-31; NMR; NMR spectroscopy;
D O I：
10.1520/STP12009S
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A series of engine oil samples collected during a study of their Phosphorus Emission Index values were analyzed by P-31 Nuclear Magnetic Resonance Spectroscopy. (The PEI analyses themselves were presented in an associated paper [1]). NMR spectra were generated to obtain and explain the mode of formation and identity of the phosphorus-containing species in the volatiles generated during the Selby-Noack volatility test and to compare these species to those found in both the fresh oil and the residual oil remaining after the volatility test.
引用
收藏
页码：255 / 273
页数：19
相关论文
共 50 条
  • [21] Determination of phospholipids in olive oil by 31P NMR Spectroscopy
    Hatzakis, Emmanuel
    Koidis, Anastasios
    Boskou, Dimitrios
    Dais, Photis
    JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2008, 56 (15) : 6232 - 6240
  • [22] Applications of solid-state 31P NMR spectroscopy
    Iuga, A.
    Ader, C.
    Groeger, C.
    Brunner, E.
    ANNUAL REPORTS ON NMR SPECTROSCOPY, VOL 60, 2007, 60 : 145 - 189
  • [23] Principles of multiparametric optimization for phospholipidomics by 31P NMR spectroscopy
    Lutz N.W.
    Cozzone P.J.
    Biophysical Reviews, 2013, 5 (4) : 295 - 304
  • [24] Quantification of mRNA Using 31P NMR Spectroscopy and CRAFT
    Khirich, Gennady
    Noreika, Vanessa A.
    Catlin, Kaitlyn Doolittle
    Napolitano, Jose G.
    Russell, David J.
    Birkholz, Oliver
    Schumacher, Jens
    Haas, Heinrich
    Skidmore, Ken
    MAGNETIC RESONANCE IN CHEMISTRY, 2025,
  • [25] Sequences of copolyesters by 1H NMR and 31P NMR spectroscopy
    Murano, M
    POLYMER JOURNAL, 1998, 30 (04) : 281 - 283
  • [26] Sequences of Copolyesters by 1H NMR and 31P NMR Spectroscopy
    Masao Murano
    Polymer Journal, 1998, 30 : 281 - 283
  • [27] Gallic acid derivatives as stabilizers in cellulose solutions: analysis by 31P NMR spectroscopy
    Johanna Zieher
    Ivan Melikhov
    Markus Bacher
    Hubert Hettegger
    Antje Potthast
    Thomas Rosenau
    Cellulose, 2023, 30 : 6109 - 6118
  • [28] Gallic acid derivatives as stabilizers in cellulose solutions: analysis by 31P NMR spectroscopy
    Zieher, Johanna
    Melikhov, Ivan
    Bacher, Markus
    Hettegger, Hubert
    Potthast, Antje
    Rosenau, Thomas
    CELLULOSE, 2023, 30 (10) : 6109 - 6118
  • [29] Analysis of the effects of thermal treatments on CaHPO4 by 31P NMR spectroscopy
    Louati, B
    Hlel, F
    Guidara, K
    Gargouri, M
    JOURNAL OF ALLOYS AND COMPOUNDS, 2005, 394 (1-2) : 13 - 18
  • [30] 31P NMR INEPT spectroscopy:: a powerful tool for structural analysis of phosphitylated carbohydrates
    Pouységu, L
    De Jéso, B
    Lartigue, JC
    Pétraud, M
    Ratier, M
    MAGNETIC RESONANCE IN CHEMISTRY, 2000, 38 (08) : 668 - 674
12345