Analysis of the volatiles generated during the Selby-Noack test by 31P NMR spectroscopy

被引：0
|
作者：
Bosch, RJ [1 ]
Fee, DC [1 ]
Selby, TW [1 ]
机构：
[1] Astaris LLC, Webster Groves, MO 63119 USA
来源：
Elemental Analysis of Fuels and Lubricants: Recent Advances and Future Prospects | 2005年 / 1468卷
关键词：
phosphorus volatility; exhaust catalyst; exhaust emissions; ZDDP; zinc dithiophosphates; phosphorus emission index; PEI; P-31; NMR; NMR spectroscopy;
D O I：
10.1520/STP12009S
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A series of engine oil samples collected during a study of their Phosphorus Emission Index values were analyzed by P-31 Nuclear Magnetic Resonance Spectroscopy. (The PEI analyses themselves were presented in an associated paper [1]). NMR spectra were generated to obtain and explain the mode of formation and identity of the phosphorus-containing species in the volatiles generated during the Selby-Noack volatility test and to compare these species to those found in both the fresh oil and the residual oil remaining after the volatility test.
引用
收藏
页码：255 / 273
页数：19
相关论文
共 50 条
  • [1] 31P NMR spectroscopy in food analysis
    Spyros, A.
    Dais, P.
    PROGRESS IN NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY, 2009, 54 (3-4) : 195 - 207
  • [2] Key chromophores in celluloses: analysis by 31P NMR spectroscopy
    Johanna Zieher
    Markus Bacher
    Irina Sulaeva
    Ivan Sumerskii
    Hubert Hettegger
    Antje Potthast
    Thomas Rosenau
    Cellulose, 2023, 30 : 5437 - 5445
  • [3] Key chromophores in celluloses: analysis by 31P NMR spectroscopy
    Zieher, Johanna
    Bacher, Markus
    Sulaeva, Irina
    Sumerskii, Ivan
    Hettegger, Hubert
    Potthast, Antje
    Rosenau, Thomas
    CELLULOSE, 2023, 30 (09) : 5437 - 5445
  • [4] 31P NMR analysis of cyclotriphosphazenes
    Wu, HS
    Meng, SS
    INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 1998, 37 (02) : 675 - 683
  • [5] Analysis of phospholipid molecular species in brain by 31P NMR spectroscopy
    Pearce, JM
    Komoroski, RA
    MAGNETIC RESONANCE IN MEDICINE, 2000, 44 (02) : 215 - 223
  • [6] Characterization of technical lignins by NMR spectroscopy: optimization of functional group analysis by 31P NMR spectroscopy
    Korntner, Philipp
    Sumerskii, Ivan
    Bacher, Markus
    Rosenau, Thomas
    Potthast, Antje
    HOLZFORSCHUNG, 2015, 69 (06) : 807 - 814
  • [7] Quantitative 31P NMR spectroscopy of humic acids
    Novák, F
    Hrabal, R
    Bartosová, I
    Kalcík, J
    CHEMICKE LISTY, 2005, 99 (04): : 236 - 245
  • [8] Phosphate kinetics during dialysis:: Modeling and study by NMR spectroscopy of 31P
    Maasrani, M
    INTERNATIONAL JOURNAL OF ARTIFICIAL ORGANS, 2006, 29 (05): : 502 - 502
  • [9] 31P NMR Spectroscopy in an Undergraduate Inorganic Curriculum
    Nataro, Chip
    Mandell, Chelsea L.
    Tiedemann, Margaret A.
    NMR SPECTROSCOPY IN THE UNDERGRADUATE CURRICULUM, 2013, 1128 : 131 - +
  • [10] Analysis of enzymatically generated phosphoinositides by 31P nuclear magnetic resonance spectroscopy
    Müller, M
    Schiller, J
    Petkovic, M
    Zschörnig, O
    Arnhold, J
    Arnold, K
    ANALYTICAL BIOCHEMISTRY, 2004, 330 (01) : 167 - 171
12345