Facile procedure to synthesize highly crystalline Ag/NiO nanocomposite microspheres and their photocatalytic activity

被引:21
作者
Chen, You-Cun [1 ,2 ]
Zheng, Fang-Cai [1 ,2 ]
Min, Yu-Lin [1 ,2 ]
Wang, Tao [1 ,2 ]
Zhang, Yuan-Guang [1 ,2 ]
Wang, Yan-Xia [1 ,2 ]
机构
[1] Anqing Normal Univ, Sch Chem & Chem Engn, Anqing 246011, Peoples R China
[2] Anqing Normal Univ, Anhui Prov Lab Optoelect & Magnetism Funct Mat, Anqing 246011, Peoples R China
基金
美国国家科学基金会;
关键词
THERMAL-DECOMPOSITION; HIERARCHICAL BETA-NI(OH)(2); MAGNETIC NANOPARTICLES; OPTICAL-PROPERTIES; NIO; TIO2; DEGRADATION; ION; AU; AG;
D O I
10.1007/s10854-012-0634-8
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
The beta-Ni(OH)(2) microspheres have been fabricated by a facile hydrothermal method in the assistance of biomolecule (l-arginine). The NiO microspheres were obtained with further calcination of beta-Ni(OH)(2) precursor at 500 A degrees C for 2 h. Subsequently, Ag/NiO nanocomposite microspheres were also prepared by the reduction of AgNO3 solution. The as-synthesized products were characterized by X-ray power diffraction, scanning electron microscopy, transmission electron microscopy, energy-dispersive X-ray spectroscopy, thermogravimetric analysis et al. The photocatalytic activity of Ag/NiO composite microspheres was also investigated by UV-Vis spectrophotometer and the results display enhanced photocatalytic activity in degradation of methyl orange.
引用
收藏
页码:1592 / 1598
页数:7
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