Ethanol-Assisted Hydrothermal Synthesis and Characterization of BiFeO3 Nanopowders

被引：19

作者：

Chen, Zhiwu ^{[1
]}

Wu, Yongpeng ^{[1
]}

Hu, Jianqiang ^{[2
]}

机构：

[1] S China Univ Technol, Coll Mat Sci & Engn, Guangzhou 510640, Guangdong, Peoples R China

[2] S China Univ Technol, Coll Chem & Chem Engn, Guangzhou 510640, Guangdong, Peoples R China

来源：

JOURNAL OF THE AMERICAN CERAMIC SOCIETY | 2013年 / 96卷 / 05期

关键词：

LOW-TEMPERATURE SYNTHESIS; THIN-FILM HETEROSTRUCTURES; NANOSIZED BISMUTH FERRITE; MAGNETIC-PROPERTIES; NANOPARTICLES; MINERALIZER; ROUTE;

D O I：

10.1111/jace.12296

中图分类号：

TQ174 [陶瓷工业]; TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

Well-crystallized pure BiFeO3 nanopowders were successfully synthesized at the temperature as low as 120 degrees C by an ethanol-assisted hydrothermal process. In this synthesis, the composition of the solvent played important roles in the formation of pure BiFeO3. The BiFeO3 nanopowders synthesized with 4:3 ethanol/water ratio mainly consists of cubic structures with size from 50 to 150nm. Zero-field-cooled (ZFC) and field-cooled (FC) magnetization measurements indicated that pure BiFeO3 nanopowders showed a spin-glass transition below the freezing temperature. Moreover, the BiFeO3 nanopowders exhibited ferromagnetic order at room temperature.

引用

页码：1345 / 1348

页数：4

共 23 条

[1] Synthesis, and study of magnetic properties, of Bi1-x Cd x FeO3 [J].

Bellakki, M. B. ;

Manivannan, V. .

JOURNAL OF MATERIALS SCIENCE, 2010, 45 (04) :1137-1142

[2] Homogeneous precipitation of cerium dioxide nanoparticles in alcohol/water mixed solvents [J].

Chen, HI ;

Chang, HY .

COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2004, 242 (1-3) :61-69

[3] Nanoscale domain control in multiferroic BiFeO3 thin films [J].

Chu, Ying-Hao ;

Zhan, Qian ;

Martin, Lane W. ;

Cruz, Maria P. ;

Yang, Pei-Ling ;

Pabst, Gary W. ;

Zavaliche, Florin ;

Yang, Seung-Yeul ;

Zhang, Jing-Xian ;

Chen, Long-Qing ;

Schlom, Darrell G. ;

Lin, I. -Nan ;

Wu, Tai-Bor ;

Ramesh, Ramamoorthy .

ADVANCED MATERIALS, 2006, 18 (17) :2307-+

[4] Nanosized bismuth ferrite powder prepared through sonochemical and microemulsion techniques [J].

Das, Nandini ;

Majumdar, Ranabrata ;

Sen, A. ;

Maiti, H. S. .

MATERIALS LETTERS, 2007, 61 (10) :2100-2104

[5] Effect of doping on the morphology and multiferroic properties of BiFeO3 nanorods [J].

Dutta, Dimple P. ;

Jayakumar, O. D. ;

Tyagi, A. K. ;

Girija, K. G. ;

Pillai, C. G. S. ;

Sharma, G. .

NANOSCALE, 2010, 2 (07) :1149-1154

[6] Multiferroic and magnetoelectric materials [J].

Eerenstein, W. ;

Mathur, N. D. ;

Scott, J. F. .

NATURE, 2006, 442 (7104) :759-765

[7] Comment on "Epitaxial BiFeO3 multiferroic thin film heterostructures" [J].

Eerenstein, W ;

Morrison, FD ;

Dho, J ;

Blamire, MG ;

Scott, JF ;

Mathur, ND .

SCIENCE, 2005, 307 (5713) :1203-1203

[8] TEMPERATURE-DEPENDENCE OF THE CRYSTAL AND MAGNETIC-STRUCTURES OF BIFEO3 [J].

FISCHER, P ;

POLOMSKA, M ;

SOSNOWSKA, I ;

SZYMANSKI, M .

JOURNAL OF PHYSICS C-SOLID STATE PHYSICS, 1980, 13 (10) :1931-1940

[9] The Synthesis of Pure-Phase Bismuth Ferrite in the Bi-Fe-O System Under Hydrothermal Conditions without a Mineralizer [J].

Gajovic, Andreja ;

Sturm, Saso ;

Jancar, Bostjan ;

Santic, Ana ;

Zagar, Kristina ;

Ceh, Miran .

JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2010, 93 (10) :3173-3179

[10] Visible-light photocatalytic properties of weak magnetic BiFeO3 nanoparticles [J].

Gao, Feng ;

Chen, Xinyi ;

Yin, Kuibo ;

Dong, Shuai ;

Ren, Zhifeng ;

Yuan, Fang ;

Yu, Tao ;

Zou, Zhigang ;

Liu, Jun-Ming .

ADVANCED MATERIALS, 2007, 19 (19) :2889-+

← 1 2 3 →