Nanoporous Titania-Supported Gold Nanoparticle-Catalyzed Green Synthesis of 1,2,3-Triazoles in Aqueous Medium

被引：68
|
作者：
Boominathan, Muthusamy [1 ]
Pugazhenthiran, Nalenthiran [2 ]
Nagaraj, Muthupandi [1 ]
Muthusubramanian, Shanmugam [1 ]
Murugesan, Sepperumal [2 ]
Bhuvanesh, Nattamai [3 ]
机构：
[1] Madurai Kamaraj Univ, Sch Chem, Dept Organ Chem, Madurai 625021, Tamil Nadu, India
[2] Madurai Kamaraj Univ, Sch Chem, Dept Inorgan Chem, Madurai 625021, Tamil Nadu, India
[3] Texas A&M Univ, Dept Chem, Xray Diffract Lab, College Stn, TX 77842 USA
来源：
ACS SUSTAINABLE CHEMISTRY & ENGINEERING | 2013年 / 1卷 / 11期
关键词：
Gold nanoparticles; Cycloaddition; Huisgen reaction; Heterogeneous catalysis; Triazole; SURFACE ORGANOMETALLIC CHEMISTRY; AZIDE-ALKYNE CYCLOADDITION; ONE-POT SYNTHESIS; 1,3-DIPOLAR CYCLOADDITION; DEPOSITION-PRECIPITATION; REGIOSELECTIVE SYNTHESIS; HETEROGENEOUS CATALYSIS; ORGANIC-REACTIONS; TERMINAL ALKYNES; CLICK CHEMISTRY;
D O I：
10.1021/sc400147r
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Nanoporous titania-supported gold nanoparprecipitation method, and the synthesized nanoparticles have been characterized by XRD, SEM, HRTEM, EDAX, BET adsorption isotherm, and IR and UV vis spectral techniques. The efficiency of this catalyst toward green organic synthesis has been studied by carrying out the 1,3-dipolar cycloaddition of organic azides with a variety of terminal alkynes in water. The reaction proceeds regioselectively yielding the corresponding 1,4-disubstituted-1,2,3-triazole derivative in good to excellent yield.
引用
收藏
页码：1405 / 1411
页数：7
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