Determination of the stereochemistry of four spirodiastereoisomers by one- and two-dimensional NOE studies

被引：0

作者：

Moreno, A ^{[1
]}

DiazOrtiz, A ^{[1
]}

DiezBarra, E ^{[1
]}

delaHoz, A ^{[1
]}

Langa, F ^{[1
]}

Prieto, P ^{[1
]}

Claridge, TDW ^{[1
]}

机构：

[1] UNIV OXFORD, DYSON PERRINS LAB, OXFORD OX1 3QY, ENGLAND

来源：

MAGNETIC RESONANCE IN CHEMISTRY | 1996年 / 34卷 / 01期

关键词：

NMR; H-1; NOE difference spectroscopy; NOESY; spiro compounds;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The stereochemistries of four cycloadducts obtained by 1,3-dipolar reactions were investigated with one- and two-dimensional NMR techniques, Analysis of a series of homonuclear NOE difference spectra and COSY and NOESY spectra recorded in a variety of solvents and at various temperatures allowed the determination of the full stereochemistry of each adduct.

引用

页码：52 / 58

页数：7

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