One-step synthesis of copper nanoparticles embedded in carbon composites

被引:17
作者
Seo, Jung Yoon [1 ]
Kang, Hyun Woo [1 ]
Jung, Dae Soo [1 ]
Lee, Hye Moon [2 ]
Park, Seung Bin [1 ]
机构
[1] Korea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Taejon 305701, South Korea
[2] KIMS, Funct Mat Div, Chang Won 641831, Gyeongnam, South Korea
基金
新加坡国家研究基金会;
关键词
Composites; Chemical synthesis; Electron microscopy; Photoelectron spectroscopy; Optical properties; SILVER NANOPARTICLES; METAL NANOPARTICLES; SIZE; GROWTH; FABRICATION; DEPENDENCE; MORPHOLOGY; POWDER; CU2O;
D O I
10.1016/j.materresbull.2012.12.070
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Copper nanoparticles embedded in carbon composites were prepared via spray pyrolysis by adjusting the polyvinylpyrrolidone (PVP) to copper nitrate mass ratio. When the equal amount of two precursors was mixed and spray pyrolyzed, copper nanoparticles with sizes in the range 30-50 nm were incorporated into the carbon composites arising from PVP. X-ray photoelectron spectroscopy demonstrated that the copper nanoparticles exhibit oxidation resistance. In addition, the effects of carbon on the surface plasmon bands were investigated. This synthetic process is simple and environmentally friendly and reduces the problems associated with their oxidation through one-step passivation. (C) 2013 Elsevier Ltd. All rights reserved.
引用
收藏
页码:1484 / 1489
页数:6
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