Sintering of titania nanoceramic: Densification and grain growth

被引:67
作者
Mazaheri, Mehdi [1 ]
Zahedi, A. M. [1 ]
Haghighatzadeh, M. [1 ]
Sadrnezhaad, S. K. [1 ]
机构
[1] Mat & Energy Res Ctr, Tehran, Iran
关键词
Sintering; Grain boundaries; TiO2; Triple junctions; Grain growth; TIO2 ANATASE CERAMICS; NANOCRYSTALLINE CERAMICS; TRIPLE JUNCTIONS; TEMPERATURE; SIZE; BEHAVIOR;
D O I
10.1016/j.ceramint.2008.02.005
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Two-step sintering (TSS) has been applied in the current study to suppress the accelerated grain growth of TiO2 nanopowder compacts in the final sintering stage. While the grain size ranges between 1 and 2 mu m in the full dense structures produced by pressureless conventional sintering (CS), application of two-step sintering has led to a remarkable grain size decline to similar to 250 nm. With regard to the expensive procedure of spark plasma sintering (SPS), similar density and grain size results determine the straightforward TSS method as a desirable rival for SPS. (C) 2008 Elsevier Ltd and Techna Group S.r.l. All fights reserved.
引用
收藏
页码:685 / 691
页数:7
相关论文
共 46 条
[1]   Spark-plasma-sintering (SPS) of nanostructured and submicron titanium oxide powders [J].
Angerer, P ;
Yu, LG ;
Khor, KA ;
Krumpel, G .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2004, 381 (1-2) :16-19
[2]  
Barbe CJ, 1997, J AM CERAM SOC, V80, P3157, DOI 10.1111/j.1151-2916.1997.tb03245.x
[3]   Sintering dense nanocrystalline ceramics without final-stage grain growth [J].
Chen, IW ;
Wang, XH .
NATURE, 2000, 404 (6774) :168-171
[4]  
CULLITY BD, 1978, DIFFRACTION, V1, P100
[5]   Influence of triple junctions on grain boundary motion [J].
Czubayko, U ;
Sursaeva, VG ;
Gottstein, G ;
Shvindlerman, LS .
ACTA MATERIALIA, 1998, 46 (16) :5863-5871
[6]   Processing and microstructure of high-pressure consolidated ceramic nanocomposites [J].
Duan, RG ;
Zhan, GD ;
Kuntz, JD ;
Kear, BH ;
Mukherjee, AK .
SCRIPTA MATERIALIA, 2004, 51 (12) :1135-1139
[7]  
German R.M., 1984, Powder Metallurgy Science
[8]  
Grätzel M, 2000, PROG PHOTOVOLTAICS, V8, P171, DOI 10.1002/(SICI)1099-159X(200001/02)8:1<171::AID-PIP300>3.0.CO
[9]  
2-U
[10]  
Groot Zevert W. F. M., 1990, Journal of Materials Science, V25, P3449, DOI 10.1007/BF00575369