A synthesis, MAS NMR, synchrotron X-ray powder diffraction, and computational study of zeolite SSZ-23

被引：36
作者：
Camblor, MA
Díaz-Cabañas, MJ
Cox, PA
Shannon, IJ
Wright, PA
Morris, RE
机构：
[1] Univ Politecn Valencia, Inst Tecnol Quim, E-46071 Valencia, Spain
[2] Univ Portsmouth, Sch Pharm & Biomed Sci, Portsmouth PO1 2DT, Hants, England
[3] Univ St Andrews, Sch Chem, St Andrews KY16 9ST, Fife, Scotland
来源：
CHEMISTRY OF MATERIALS | 1999年 / 11卷 / 10期
关键词：
D O I：
10.1021/cm991057r
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
The zeolite SSZ-23 (STT) is the first zeolite found to contain channels bounded by seven and nine tetrahedral atom windows. A survey of the synthetic conditions needed to prepare SSZ-23 has been carried out, and the resulting materials characterized by synchrotron X-ray powder diffraction and magic-angle spinning NMR spectroscopy to obtain details of the long-range crystalline structure and short-range connectivity defects. The lattice energy minimized structure is in excellent agreement with the experimental results, and a comparison with other zeolites that have been simulated in this way is made.
引用
收藏
页码：2878 / 2885
页数：8
相关论文
共 50 条
  • [1] Synchrotron X-ray diffraction, neutron diffraction, 29Si MAS-NMR, and computational study of the siliceous form of zeolite ferrierite
    [J]. 1600, (116):
  • [2] Synchrotron X-ray powder diffraction and computational investigation of purely siliceous zeolite Y under pressure
    [J]. Hriljac, J.A. (j.a.hriljac@bham.ac.uk), 1600, American Chemical Society (126):
  • [3] Synchrotron X-ray powder diffraction and computational investigation of purely siliceous zeolite Y under pressure
    Colligan, M
    Forster, PM
    Cheetham, AK
    Lee, Y
    Vogt, T
    Hriljac, JA
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2004, 126 (38) : 12015 - 12022
  • [4] A SYNCHROTRON X-RAY-DIFFRACTION, NEUTRON-DIFFRACTION, SI-29 MAS-NMR, AND COMPUTATIONAL STUDY OF THE SILICEOUS FORM OF ZEOLITE FERRIERITE
    MORRIS, RE
    WEIGEL, SJ
    HENSON, NJ
    BULL, LM
    JANICKE, MT
    CHMELKA, BF
    CHEETHAM, AK
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1994, 116 (26) : 11849 - 11855
  • [5] The dehydration process in the zeolite laumontite: A real-time synchrotron X-ray powder diffraction study
    Stahl, K
    Artioli, G
    Hanson, JC
    [J]. PHYSICS AND CHEMISTRY OF MINERALS, 1996, 23 (06) : 328 - 336
  • [6] Study of the initial stage of zeolite a synthesis by dynamic light scattering and synchrotron X-ray diffraction
    Carotenuto, L
    Piccolo, C
    Artioli, G
    Norby, P
    Grizzetti, R
    [J]. PHOTON CORRELATION AND SCATTERING, TECHNICAL DIGEST, 2000, 47 : 86 - 88
  • [7] A HIGH-RESOLUTION NMR AND SYNCHROTRON X-RAY-POWDER DIFFRACTION STUDY OF ZEOLITE ZSM-11
    TOBY, BH
    EDDY, MM
    FYFE, CA
    KOKOTAILO, GT
    STROBL, H
    COX, DE
    [J]. JOURNAL OF MATERIALS RESEARCH, 1988, 3 (03) : 563 - 569
  • [8] Industrial aspects of synchrotron X-ray powder diffraction
    [J]. Radiat Phys Chem, 3 (445):
  • [9] Synchrotron X-ray powder diffraction data of atorvastatin
    Antonio, Selma Gutierrez
    Benini, Fernanda Ribeiro
    Ferreira, Fabio Furlan
    Pires Rosa, Paulo Cesar
    Paiva-Santos, Carlos de Oliveira
    [J]. POWDER DIFFRACTION, 2008, 23 (04) : 350 - 355
  • [10] In situ dynamic light scattering and synchrotron, X-ray powder diffraction study of the early stages of zeolite growth
    Artioli, G
    Grizzetti, R
    Carotenuto, L
    Piccolo, C
    Colella, C
    Liguori, B
    Aiello, R
    Frontera, P
    [J]. IMPACT OF ZEOLITES AND OTHER POROUS MATERIALS ON THE NEW TECHNOLOGIES AT THE BEGINNING OF THE NEW MILLENNIUM, PTS A AND B, 2002, 142 : 45 - 52
12345