(E)-3-(3,4-Dimethoxyphenyl)-1-(2-thienyl)prop-2-en-1-one

被引：0

作者：

Fun, Hoong-Kun ^{[1
]}

Jebas, Samuel Robinson ^{[1
]}

Patil, P. S. ^{[2
]}

Dharmaprakash, S. M. ^{[2
]}

机构：

[1] Univ Sains Malaysia, Sch Phys, Xray Crystallog Unit, George Town 11800, Malaysia

[2] Mangalore Univ, Dept Studies Phys, Mangalore 574199, India

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2008年 / 64卷

关键词：

D O I：

10.1107/S1600536808020631

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C15H14O3S, has two symmetry-independent molecules in the asymmetric unit with almost identical geometry. The dihedral angle between the benzene and thiophene rings is 1.61 (11)degrees in one molecule and 7.21 (11)degrees in the other. In both molecules, C-H center dot center dot center dot O hydrogen bonds generate rings of graph-set motif S(5). The crystal structure is stabilized by C-H center dot center dot center dot O hydrogen bonds, C-H center dot center dot center dot pi interactions and pi-pi interactions involving the benzene and thiophene rings, with centroid-centroid distances of 3.5249 (13) and 3.6057 (13) angstrom.

引用

页码：O1440 / U1802

页数：12

共 10 条

[1] Second-order nonlinear optical susceptibility in chalcone-group crystalline molecular compounds
Agrinskaya, NV
Lukoshkin, VA
Kudryavtsev, VV
Nosova, GI
Solovskaya, NA
Yakimanskii, AV
[J]. PHYSICS OF THE SOLID STATE, 1999, 41 (11) : 1914 - 1917
[2] TABLES OF BOND LENGTHS DETERMINED BY X-RAY AND NEUTRON-DIFFRACTION .1. BOND LENGTHS IN ORGANIC-COMPOUNDS
ALLEN, FH
KENNARD, O
WATSON, DG
BRAMMER, L
ORPEN, AG
TAYLOR, R
[J]. JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1987, (12): : S1 - S19
[3] PATTERNS IN HYDROGEN BONDING - FUNCTIONALITY AND GRAPH SET ANALYSIS IN CRYSTALS
BERNSTEIN, J
DAVIS, RE
SHIMONI, L
CHANG, NL
[J]. ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 1995, 34 (15) : 1555 - 1573
[4] Bruker, 2005, APEX2 SAINT SADABS
[5] A series of substituted (2E)-3-(2-fluoro-4-phenoxyphenyl)-1-phenyl-prop-2-en-1-ones
Chopra, Deepak
Mohan, T. P.
Vishalakshi, B.
Row, T. N. Guru
[J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2007, 63 : O704 - O710
[6] 1-(4-Chlorophenyl)-3-(4-ethoxyphenyl)-prop-2-en-1-one
Patil, P. S.
Fun, Hoong-Kun
Chantrapromma, Suchada
Dharmaprakash, S. M.
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O2497 - O2498
[7] 3-(5-Bromo-2-thienyl)-1-(4-methoxyphenyl)-prop-2-en-1-one
Patil, P. S.
Ng, Shea-Lin
Razak, Ibrahim Abdul
Fun, Hoong-Kun
Dharmaprakash, S. M.
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O59 - O60
[8] 3-(4-Methoxyphenyl)-1-(4-nitrophenyl)prop-2-en-1-one
Patil, PS
Teh, JBJ
Fun, HK
Razak, IA
Dharmaprakash, SM
[J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2006, 62 : O896 - O898
[9] A short history of SHELX
Sheldrick, George M.
[J]. ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 : 112 - 122
[10] Single-crystal structure validation with the program PLATON
Spek, AL
[J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2003, 36 : 7 - 13

← 1 →