Investigation of the purity of antimony pentafluoride using 19F NMR

被引：5

作者：

Bock, A. ^{[1
,2
]}

Dubois, M. ^{[1
,2
]}

Bonnet, P. ^{[1
,2
]}

Hamwi, A. ^{[1
,2
]}

Avignant, D. ^{[1
,2
]}

Moch, L.

Morel, B.

机构：

[1] Univ Clermont Ferrand, Clermont Univ, Lab Mat Inorgan, F-63171 Aubiere, France

[2] CNRS, UMR 6002, F-63170 Aubiere, France

来源：

JOURNAL OF FLUORINE CHEMISTRY | 2012年 / 134卷

关键词：

Antimony; Pentafluoride; Fluoride; SbF5; Fluorination; F-19; NMR;

D O I：

10.1016/j.jfluchem.2011.05.002

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Samples of antimony pentafluoride from different syntheses as well as commercial products were investigated by F-19 and H-1 NMR and compared. HF was identified as impurity and SbF6- specie is also present. Their amounts have been correlated through a method based on F-19 NMR. (C) 2011 Elsevier B.V. All rights reserved.

引用

页码：24 / 28

页数：5

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