Synthesis and characterization of WO3 nanowires and metal nanoparticle-WO3 nanowire composites

被引:24
作者
Szabo, Maria [1 ]
Pusztai, Peter [1 ]
Leino, Anne-Riikka [2 ]
Kordas, Krisztian [2 ]
Konya, Zoltan [1 ,3 ]
Kukovecz, Akos [1 ,4 ]
机构
[1] Univ Szeged, Dept Appl & Environm Chem, H-6720 Szeged, Hungary
[2] Univ Oulu, Dept Elect & Informat Engn, Microelect & Mat Phys Labs, F1-90014 Oulu, Finland
[3] MTA SZTE React Kinet & Surface Chem Res Grp, H-6720 Szeged, Hungary
[4] MTA SZTE Lendulet Porous Nanocomposites Res Grp, H-6720 Szeged, Hungary
关键词
Tungsten-trioxide; Hydrothermal; Metal decoration; Electron microscopy; Spectrometry; NANOTUBES;
D O I
10.1016/j.molstruc.2012.11.041
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Tungsten-trioxide nanowire bundles were prepared using a simple hydrothermal method. Sodium-tungstate was used as precursor and sodium-sulfate as structure directing agent. All the reflections of the Xray diffractogram of the synthesized wires belong to the hexagonal phase of the tungsten trioxide. The nanowires were successfully decorated with metal nanoparticles by wet impregnation. The TEM investigation showed that using different metal precursors resulted in different particle sizes and coverage on the surface. (C) 2012 Elsevier B.V. All rights reserved.
引用
收藏
页码:99 / 103
页数:5
相关论文
共 32 条
[1]   Enhancement of photocatalytic and electrochromic properties of electrochemically fabricated mesoporous WO3 thin films [J].
Baeck, SH ;
Choi, KS ;
Jaramillo, TF ;
Stucky, GD ;
McFarland, EW .
ADVANCED MATERIALS, 2003, 15 (15) :1269-+
[2]   The visible light induced photocatalytic activity of tungsten trioxide powders [J].
Bamwenda, GR ;
Arakawa, H .
APPLIED CATALYSIS A-GENERAL, 2001, 210 (1-2) :181-191
[3]   Hydrothermal technology for nanotechnology [J].
Byrappa, K. ;
Adschiri, T. .
PROGRESS IN CRYSTAL GROWTH AND CHARACTERIZATION OF MATERIALS, 2007, 53 (02) :117-166
[4]  
BYRAPPA K, 2001, HDB HYDROTHERMAL TEC, pCH1
[5]  
Cui H. N., 2005, THESIS U MINHO
[6]   Metal oxide nano-particles for improved electrochromic and lithium-ion battery technologies [J].
Dillon, A. C. ;
Mahan, A. H. ;
Deshpande, R. ;
Parilla, Ra. ;
Jones, K. M. ;
Lee, S-H. .
THIN SOLID FILMS, 2008, 516 (05) :794-797
[7]  
Flynn T., 2005, BIOL MED, V1, P150
[8]   High-activity, single-site mesoporous WO3-MCF materials for the catalytic epoxidation of cycloocta-1,5-diene with aqueous hydrogen peroxide [J].
Gao, Ruihua ;
Yang, Xinli ;
Dai, Wei-Lin ;
Le, Yingyi ;
Li, Hexing ;
Fan, Kangnian .
JOURNAL OF CATALYSIS, 2008, 256 (02) :259-267
[9]  
Gibson JM, 1997, PHYS TODAY, V50, P56, DOI 10.1063/1.881964
[10]  
HEALTH JR, 1993, CHEM PHYS LETT, V208, P263