Synthesis of metal selenide colloidal nanocrystals by the hot injection of selenium powder

被引：14

作者：

Flamee, Stijn ^{[1
,2
,3
]}

Dierick, Ruben ^{[1
,2
,4
]}

Cirillo, Marco ^{[1
,2
]}

Van Genechten, Dirk ^{[3
]}

Aubert, Tangi ^{[1
,2
]}

Hens, Zeger ^{[1
,2
]}

机构：

[1] Univ Ghent, B-9000 Ghent, Belgium

[2] Univ Ghent, Ctr Nano & Biophoton, B-9000 Ghent, Belgium

[3] Umicore Grp Res & Dev, B-2250 Olen, Belgium

[4] Mat Program SoPPoM, Strateg Initiat, Ghent, Belgium

来源：

DALTON TRANSACTIONS | 2013年 / 42卷 / 35期

关键词：

LIGHT-EMITTING-DIODES; SOLAR-CELLS; SURFACE-CHEMISTRY; SHAPE-EVOLUTION; SCALE SYNTHESIS; CDSE; CUINSE2; SIZE; INKS;

D O I：

10.1039/c3dt50757b

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

We describe the synthesis of metal selenide nanocrystals, including CdSe, ZnSe, CuInSe2 and Cu-2(Zn, Sn)-Se-4, by the hot injection of selenium powder dispersed in a carrier solvent. Since this results in a fast and high yield nanocrystal formation, we argue that the approach is well suited for the low cost, large volume production of nanocrystals.

引用

页码：12654 / 12661

页数：8

共 57 条

[1] Tuning the Postfocused Size of Colloidal Nanocrystals by the Reaction Rate: From Theory to Application [J].

Abe, Sofie ;

Capek, Richard Karel ;

De Geyter, Bram ;

Hens, Zeger .

ACS NANO, 2012, 6 (01) :42-53

[2] Inkjet-printed nanocrystal photodetectors operating up to 3 μm wavelengths [J].

Boeberl, Michaela ;

Kovalenko, Maksym V. ;

Gamerith, Stefan ;

List, Emil J. W. ;

Heiss, Wolfgang .

ADVANCED MATERIALS, 2007, 19 (21) :3574-+

[3] SYNTHESIS OF THIOL-DERIVATIZED GOLD NANOPARTICLES IN A 2-PHASE LIQUID-LIQUID SYSTEM [J].

BRUST, M ;

WALKER, M ;

BETHELL, D ;

SCHIFFRIN, DJ ;

WHYMAN, R .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1994, (07) :801-802

[4] High Activity Phosphine-Free Selenium Precursor Solution for Semiconductor Nanocrystal Growth [J].

Bullen, Craig ;

van Embden, Joel ;

Jasieniak, Jacek ;

Cosgriff, Joanna E. ;

Mulder, Roger J. ;

Rizzardo, Ezio ;

Gu, Min ;

Raston, Colin L. .

CHEMISTRY OF MATERIALS, 2010, 22 (14) :4135-4143

[5] Optical Properties of Zincblende Cadmium Selenide Quantum Dots [J].

Capek, Richard Karel ;

Moreels, Iwan ;

Lambert, Karel ;

De Muynck, David ;

Zhao, Qiang ;

Vantomme, Andre ;

Vanhaecke, Frank ;

Hens, Zeger .

JOURNAL OF PHYSICAL CHEMISTRY C, 2010, 114 (14) :6371-6376

[6] Synthesis and micrometer-scale assembly of colloidal CdSe/CdS nanorods prepared by a seeded growth approach [J].

Carbone, Luigi ;

Nobile, Concetta ;

De Giorgi, Milena ;

Sala, Fabio Delia ;

Morello, Giovanni ;

Pompa, Pierpaolo ;

Hytch, Martin ;

Snoeck, Etienne ;

Fiore, Angela ;

Franchini, Isabella R. ;

Nadasan, Monica ;

Silvestre, Albert F. ;

Chiodo, Letizia ;

Kudera, Stefan ;

Cingolani, Roberto ;

Krahne, Roman ;

Manna, Liberato .

NANO LETTERS, 2007, 7 (10) :2942-2950

[7] Colloidal quantum-dot light-emitting diodes with metal-oxide charge transport layers [J].

Caruge, J. M. ;

Halpert, J. E. ;

Wood, V. ;

Bulovic, V. ;

Bawendi, M. G. .

NATURE PHOTONICS, 2008, 2 (04) :247-250

[8] Electroluminescence from single monolayers of nanocrystals in molecular organic devices [J].

Coe, S ;

Woo, WK ;

Bawendi, M ;

Bulovic, V .

NATURE, 2002, 420 (6917) :800-803

[9] Reversible Tunability of the Near-Infrared Valence Band Plasmon Resonance in Cu2-xSe Nanocrystals [J].

Dorfs, Dirk ;

Haertling, Thomas ;

Miszta, Karol ;

Bigall, Nadja C. ;

Kim, Mee Rahn ;

Genovese, Alessandro ;

Falqui, Andrea ;

Povia, Mauro ;

Manna, Liberato .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2011, 133 (29) :11175-11180

[10] Large-Scale Colloidal Synthesis of Non-Stoichiometric Cu2ZnSnSe4 Nanocrystals for Thermoelectric Applications [J].

Fan, Feng-Jia ;

Wang, Yi-Xiu ;

Liu, Xiao-Jing ;

Wu, Liang ;

Yu, Shu-Hong .

ADVANCED MATERIALS, 2012, 24 (46) :6158-6163

← 1 2 3 4 5 6 →