Identification of additive components in powdered milk by NIR imaging methods

被引:30
作者
Huang, Yue [1 ,2 ]
Min, Shungeng [1 ]
Duan, Jia [1 ]
Wu, Lijun [1 ]
Li, Qianqian [1 ]
机构
[1] China Agr Univ, Coll Sci, Beijing 100193, Peoples R China
[2] Third Class Tobacco Supervis Stn, Beijing 101121, Peoples R China
基金
中国国家自然科学基金;
关键词
Powdered milk; Near-infrared imaging; Melamine; Semi-quantification; NEAR-INFRARED SPECTROSCOPY; DOSAGE FORMS; QUALITY; FAT;
D O I
10.1016/j.foodchem.2013.06.116
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
The express assay of excessive additives in powdered milk is of vital necessity, especially during industrial production. Near-infrared microscopy provides chemical information on the spatial distribution and cluster side of components in milk-based products when materials are mixed together. Distributions of two additive components and one banned chemical in powdered milk were simulated in this study. The distribution of inorganic additive ZnSO4 was identified using the relationship imaging mode. The distribution image of lactose was obtained by assigning the wavenumber region and by using principal component analysis coupled with correlation coefficient imaging. In addition, classical least square regression was employed to quantify the banned additive, melamine, in the powdered milk. Lastly, the detection limit of melamine in powdered milk was determined using the relationship imaging mode. (C) 2013 Elsevier Ltd. All rights reserved.
引用
收藏
页码:278 / 283
页数:6
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