Synthesis and properties of iron ferrofluids

被引：62

作者：

Butter, K ^{[1
]}

Philipse, AP ^{[1
]}

Vroege, GJ ^{[1
]}

机构：

[1] Univ Utrecht, Debye Inst, Vant Hoff Lab Phys & Colloid Chem, NL-3584 CH Utrecht, Netherlands

来源：

JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS | 2002年 / 252卷 / 1-3期

关键词：

iron colloids; synthesis; transmission electron microscopy; small angle X-ray scattering; oxidation;

D O I：

10.1016/S0304-8853(02)00620-0

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

We study the preparation and properties of metallic iron particles, synthesized by thermal decomposition of Fe(CO)(5) in the presence of a stabilizer. By varying the iron carbonyl/polymer ratio, the particle size can be varied from 2 to 10nm. Particles are characterized by magnetization measurements, transmission electron microscopy (TEM), small angle X-ray scattering and cryo-TEM. Cryo-TEM pictures show linear structures of particles. From susceptibility measurements, it is seen that particles oxidize fast on exposure to air. (C) 2002 Elsevier Science B.V. All rights reserved.

引用

页码：1 / 3

页数：3

共 4 条

[1] STRUCTURE, MAGNETIC CHARACTERIZATION, AND OXIDATION OF COLLOIDAL IRON DISPERSIONS
GRIFFITHS, CH
OHORO, MP
SMITH, TW
[J]. JOURNAL OF APPLIED PHYSICS, 1979, 50 (11) : 7108 - 7115
[2] PREPARATION OF AQUEOUS MAGNETIC LIQUIDS IN ALKALINE AND ACIDIC MEDIA
MASSART, R
[J]. IEEE TRANSACTIONS ON MAGNETICS, 1981, 17 (02) : 1247 - 1248
[3] Pathmamanoharan C, 2000, PROG COLL POL SCI S, V115, P141
[4] COLLOIDAL IRON DISPERSIONS PREPARED VIA THE POLYMER-CATALYZED DECOMPOSITION OF IRON PENTACARBONYL
SMITH, TW
WYCHICK, D
[J]. JOURNAL OF PHYSICAL CHEMISTRY, 1980, 84 (12) : 1621 - 1629

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