3-Dimensional structures of open-pores in PEO films on AZ31 Mg alloy

被引:20
作者
Moon, Sungmo [1 ,2 ]
Arrabal, Raul [3 ]
Matykina, Endzhe [3 ]
机构
[1] Korea Inst Mat Sci, Surface Engn Div, Daejeon, South Korea
[2] Korea Univ Sci & Technol UST, Adv Mat Engn, Daejeon, South Korea
[3] Univ Complutense, Fac Ciencias Quim, Dept Ciencia Mat, E-28040 Madrid, Spain
关键词
Open-pore; Anodic oxide coating; PEO film; Epoxy replica; Mg alloy; PLASMA ELECTROLYTIC OXIDATION; MICRO-ARC OXIDATION; CORROSION-RESISTANCE; MAGNESIUM; ALUMINUM; PHOSPHATE; BEHAVIOR;
D O I
10.1016/j.matlet.2015.08.149
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this work, observation of 3-dimensional network structure of open-pores in plasma electrolytic oxidation (PEO) films is reported for the first time using a resin replica method. Conventional plane and cross-sectional views of PEO films provide only 2-dimensional information on the shape and size of pores in PEO films, while an epoxy replica, which was prepared by infiltrating a mixture of liquid epoxy resin and hardener into the open-pores in PEO films under high vacuum and hardening at room temperature, rendered clearly 3-dimensional information about the shape, size and position of open-pores in PEO films. The resin replica method, applied to PEO films on AZ31 Mg alloy formed in phosphate solution, revealed not only 3-dimensional network structures of irregular shape of large size and small size pores, in the middle part and near the film/alloy interface, respectively, but also spherical pores connected to the surface through narrow channels. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码:439 / 441
页数:3
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