Synthesis of 3-methylquinazolin-4(3H)-one derivatives

被引：4

作者：

Lezina, O. M. ^{[1
]}

Rubtsova, S. A. ^{[1
]}

Polukeev, V. A. ^{[2
]}

Kutchin, A. V. ^{[1
]}

机构：

[1] Russian Acad Sci, Inst Chem, Ural Div, Komi Res Ctr, Syktyvkar 167982, Russia

[2] Vekton Closed Corp, St Petersburg, Russia

来源：

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2012年 / 48卷 / 09期

关键词：

OXIDATION; THIOLS;

D O I：

10.1134/S1070428012090126

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Oxidation of 3-methyl-2-sulfanylquinazolin-4(3H)-one with chlorine dioxide under different conditions gave 2,2'-disulfanediylbis[3-methylquinazolin-4(3H)-one], 3-methyl-4-oxo-3,4-dihydroquinazoline-2-sulfonic acid, 3-methylquinazoline-2,4(1H,3H)-dione, 6-chloro-3-methylquinazoline-2,4(1H,3H)-dione, and N,N-diethyl-3-methyl-4-oxo-3,4-dihydroquinazoline-2-sulfonamide.

引用

页码：1222 / 1225

页数：4

共 10 条

[1] RADICAL IONS .89. SINGLE-ELECTRON OXIDATION OF DIARYLDISULFIDES WITH ALCL3/H2CCL2 [J].

BOCK, H ;

RITTMEYER, P .

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 1992, 68 (1-4) :261-291

[2] Traceless synthesis of quinazoline-2,4-diones by curtius rearrangement reaction using poly(ethylene glycol) as soluble - polymeric support [J].

Huang, Yanling ;

Lu, Cuifen ;

Chen, Zuxing ;

Yang, Guichun .

JOURNAL OF HETEROCYCLIC CHEMISTRY, 2007, 44 (06) :1421-1424

[3] New synthesis of alkane- and arylsulfonyl chlorides by oxidation of thiols and disulfides with chlorine dioxide [J].

Lezina, O. M. ;

Rubtsova, S. A. ;

Kuchin, A. V. .

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2011, 47 (08) :1249-1251

[4]

Lezina O.M., 2006, RU Patent, Patent No. [2302407, 2 302 407]

[5]

Lezina O.M., 2003, IZV AKAD NAUK K, P1779

[6] PREPARATION AND REARRANGEMENT REACTIONS OF A 3,1,4-BENZODIAZEPINE [J].

METLESICS, W ;

SILVERMA.G ;

STERNBAC.LH .

MONATSHEFTE FUR CHEMIE, 1967, 98 (03) :633-+

[7]

Shtephan ED, 1996, USP KHIM+, V65, P326

[8]

[Судариков Д.В. Sudarikov D.V.], 2008, [Известия высших учебных заведений. Серия: Химия и химическая технология, Izvestiya vysshikh uchebnykh zavedenii. Seriya: Khimiya i khimicheskaya tekhnologiya], V51, P112

[9]

Tumanova T.A., 1972, FIZIKOKHIMICHESKIE O, P236

[10]

Zefirov N.S., 1999, KHIMICHESKAYA ENTSIK, V5, P264

← 1 →