Spectroscopic (FT-IR, FT-Raman, 1H, 13C NMR, UV/VIS), thermogravimetric and antimicrobial studies of Ca(II), Mn(II), Cu(II), Zn(II) and Cd(II) complexes of ferulic acid

被引：68

作者：

Kalinowska, M. ^{[1
]}

Piekut, J. ^{[1
]}

Bruss, A. ^{[2
]}

Follet, C. ^{[2
]}

Sienkiewicz-Gromiuk, J. ^{[3
]}

Swislocka, R. ^{[1
]}

Rzaczynska, Z. ^{[3
]}

Lewandowski, W. ^{[1
]}

机构：

[1] Bialystok Tech Univ, Div Chem, PL-15435 Bialystok, Poland

[2] Univ Valenciennes & Hainaut Cambresis, Lab Mat Ceram & Proc Associes LMCPA EA 2443, F-59313 Valenciennes, France

[3] Marie Curie Sklodowska Univ, Dept Gen & Coordinat Chem, Lublin, Poland

来源：

SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY | 2014年 / 122卷

关键词：

Metal; 4-hydroxy-3-methoxycinnamates; FT-IR; FT-Raman; C-13 and H-1 NMR; Antimicrobiological activity; ANTIBACTERIAL ACTIVITY; CRYSTAL-STRUCTURE;

D O I：

10.1016/j.saa.2013.11.089

中图分类号：

O433 [光谱学];

学科分类号：

0703 ; 070302 ;

摘要：

The molecular structure of Mn(II), Cu(II), Zn(II), Cd(II) and Ca(II) ferulates (4-hydroxy-3-methoxycinnamates) was studied. The selected metal ferulates were synthesized. Their composition was established by means of elementary and thermogravimetric analysis. The following spectroscopic methods were used: infrared (FT-IR), Raman (FT-Raman), nuclear magnetic resonance (C-13, H-1 NMR) and ultraviolet-visible (UV/VIS). On the basis of obtained results the electronic charge distribution in studied metal complexes in comparison with ferulic acid molecule was discussed. The microbiological study of ferulic acid and ferulates toward Escherichia coli, Bacillus subtilis, Candida albicans, Pseudomonas aeruginosa, Staphylococcus aureus and Proteus vulgaris was done. (C) 2013 Elsevier B.V. All rights reserved.

引用

页码：631 / 638

页数：8

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