A straightforward synthesis of 1,2-dihydronaphtho[2,1-b]furans from 2-naphthols

被引：0
|
作者：
Arrault, A [1 ]
Touzeau, F [1 ]
Guillaumet, G [1 ]
Mérour, JY [1 ]
机构：
[1] Univ Orleans, CNRS, Inst Chim Organ & Analyt, F-45067 Orleans 2, France
来源：
SYNTHESIS-STUTTGART | 1999年 / 07期
关键词：
2-naphthols; ethyl 1,2-dihydronaphtho[2,1-b]furan-2-carboxylates; aromatization; 1,2-dihydronaphtho [2,1-b]furan-2-carbonitrile; 1-(1,2-dihydronaphtho[2,1-b]furan-2-yl)ethan-1-one;
D O I：
暂无
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A one-step synthesis of ethyl 1,2-dihydronaphtho[2,1-b]furan-2-carboxylates 2a-g from substituted 2-naphthols and ethyl 2,3-dibromopropanoate is described. 3,4-Dibromobutan-2-one and 2-chloroacrylonitrile react with 2-naphthol (1a) to afford the corresponding 2-cyano- or 2-acetylnaphtho[2,1-b]furans 6 and 7, respectively.
引用
收藏
页码：1241 / 1245
页数：5
相关论文
共 7 条
  • [1] Novel and convenient synthesis of 1-(pyridinylmethyl)-2-naphthols and 1-(pyridinylmethylene)-2-tetralones from 2-tetralones
    Po-Jung J. Huang
    Elizabeth Potter
    Amitabh Jha
    Molecular Diversity, 2010, 14 : 393 - 400
  • [2] Novel and convenient synthesis of 1-(pyridinylmethyl)-2-naphthols and 1-(pyridinylmethylene)-2-tetralones from 2-tetralones
    Huang, Po-Jung J.
    Potter, Elizabeth
    Jha, Amitabh
    MOLECULAR DIVERSITY, 2010, 14 (02) : 393 - 400
  • [3] Convenient, tandem and one-reaction vessel synthesis of mixed dialkylated 2-naphthols from 2-tetralone
    Jha, A
    Dimmock, JR
    CANADIAN JOURNAL OF CHEMISTRY, 2003, 81 (04) : 293 - 296
  • [4] A convenient one-pot synthesis of 2,2-Dialkyl-2,3-dihydro-1H-naphtho[2,1-b]pyrans
    Jha, Amitabh
    Huang, Po-Jung Jimmy
    Mukherjee, Chandrani
    Paul, Nawal K.
    SYNLETT, 2007, (20) : 3127 - 3130
  • [5] Synthesis of benzo[b]indeno[2,1-d]furanone skeleton from ninhydrin and cyclohexane-1,3-dione derivatives
    Na, JE
    Kim, JM
    Lee, SK
    Kim, JN
    BULLETIN OF THE KOREAN CHEMICAL SOCIETY, 2003, 24 (12): : 1725 - 1726
  • [6] Synthesis of new aromatic pyrrolo[2,1-c][1,4]benzodiazepines and pyrrolo[1,2-a]thieno[3,2-e][1,4]diazepines as anti-tumoral agents
    Lisowski, V
    Fabis, F
    Pierré, A
    Caignard, DH
    Renard, P
    Rault, S
    JOURNAL OF ENZYME INHIBITION AND MEDICINAL CHEMISTRY, 2002, 17 (06) : 403 - 407
  • [7] Synthesis and crystal structures of 2-methyl-4-aryl-5-oxo-5H-indeno [1,2-b] pyridine carboxylate derivatives
    Pandian, Ramesh
    Naushad, Edayadulla
    Vijayakumar, Vinodhkumar
    Peters, Guenther H.
    Nanjappagounder, Ponnuswamy Mondikalipudur
    CHEMISTRY CENTRAL JOURNAL, 2014, 8
1