Formation and crystal structure of bis-(2,2,6,6-tetramethylpiperidino)diselane

被引：1

作者：

Vojinovic, K ^{[1
]}

Mitzel, NW ^{[1
]}

机构：

[1] Univ Munster, Inst Anorgan & Analyt Chem, D-48149 Munster, Germany

来源：

INORGANICA CHIMICA ACTA | 2005年 / 358卷 / 14期

关键词：

selenium; cyclic amines; crystal structure; diaminodiselane;

D O I：

10.1016/j.ica.2005.05.031

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The reaction of N-lithioselenido-2,2,6,6-tetramethylpiperidine and trimethyltin chloride leads to the formation of hexamethyl-distannane and bis-(2,2,6,6-tetramethyl-piperidino)diselane. This compound was identified by H-1 and C-13 NMR, by mass spectrometry and elemental analysis. The crystal structure was also determined showing a conformation differing from other dian-tinodiselanes due to the repulsion of the bulky 2,2,6,6-tetramethyl-piperidino groups. (c) 2005 Elsevier B.V. All rights reserved.

引用

页码：4403 / 4406

页数：4

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