Synthesis of ZSM-12 Zeolites with New Templates Based on Salts of Ethanolamines

被引:12
|
作者
Tsaplin, D. E. [1 ]
Makeeva, D. A. [1 ]
Kulikov, L. A. [1 ,2 ]
Maksimov, A. L. [1 ,2 ]
Karakhanov, E. A. [1 ]
机构
[1] Lomonosov Moscow State Univ, Moscow 119991, Russia
[2] Russian Acad Sci, Topchiev Inst Petrochem Synth, Moscow 119991, Russia
关键词
zeolites; ZSM-12; ethanolamines; hydrothermal synthesis; CATALYTIC-PROPERTIES; AL; CRYSTALLIZATION; MORPHOLOGY;
D O I
10.1134/S1070427218120066
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
New class of templates, ethanolamine salts, was used to synthesize zeolites with the ZSM-12 structure. The materials obtained were characterized by methods of powder X-ray diffraction, scanning electron microscopy, IR spectroscopy, low-temperature adsorption-desorption of nitrogen, and elemental analysis. It was shown that, with these templates, it is possible to obtain crystallites with well formed acicular shape, hexagonal morphology, large surface area, and narrow pore size distribution.
引用
收藏
页码:1957 / 1962
页数:6
相关论文
共 28 条
  • [1] Synthesis of ZSM-12 Zeolites with New Templates Based on Salts of Ethanolamines
    D. E. Tsaplin
    D. A. Makeeva
    L. A. Kulikov
    A. L. Maksimov
    E. A. Karakhanov
    Russian Journal of Applied Chemistry, 2018, 91 : 1957 - 1962
  • [2] Disproportionation of Toluene on ZSM-12 Zeolites
    D. E. Tsaplin
    V. A. Ostroumova
    D. N. Gorbunov
    L. A. Kulikov
    E. R. Naranov
    S. V. Egazar’yants
    Russian Journal of Applied Chemistry, 2022, 95 : 1767 - 1775
  • [3] Disproportionation of Toluene on ZSM-12 Zeolites
    Tsaplin, D. E.
    Ostroumova, V. A.
    Gorbunov, D. N.
    Kulikov, L. A.
    Naranov, E. R.
    Egazar'yants, S. V.
    RUSSIAN JOURNAL OF APPLIED CHEMISTRY, 2022, 95 (12) : 1767 - 1775
  • [4] Synthesis, structure, and acidity regulation of ZSM-12 zeolite in alkane isomerization
    Shen, Yuge
    Qiao, Liang
    Zhang, Zhenli
    Gao, Shanbin
    Han, Yang
    Liu, Jixing
    Liu, Jian
    FUEL, 2025, 380
  • [5] Effects of adding alcohols on ZSM-12 synthesis
    Jegatheeswaran, Sinthuran
    Cheng, Chin-Min
    Cheng, Chil-Hung
    MICROPOROUS AND MESOPOROUS MATERIALS, 2015, 201 : 24 - 34
  • [6] A first-principles study on Pd modified ZSM-12 zeolites
    Feng, Gang
    Yang, Jinmei
    Wang, Changqing
    Lu, Kun
    Zhou, Jian
    Liu, Jianwen
    Wang, Xuewen
    Zhang, Rongbin
    Zhang, Ning
    MICROPOROUS AND MESOPOROUS MATERIALS, 2018, 260 : 227 - 234
  • [7] Role of crystal growth modifiers in the synthesis of ZSM-12 zeolite
    Sanhoob, Mohammed A.
    Muraza, Oki
    Al-Mutairi, Eid M.
    Ullah, Nisar
    ADVANCED POWDER TECHNOLOGY, 2015, 26 (01) : 188 - 192
  • [8] Microporous mesoporous ZSM-12 zeolites: Synthesis by using a soft template and textural, acid and catalytic properties
    Carvalho, Kele T. G.
    Urquieta-Gonzalez, Ernesto A.
    CATALYSIS TODAY, 2015, 243 : 92 - 102
  • [9] TEABr directed synthesis of ZSM-12 and its NMR characterization
    Yoo, K
    Kashfi, R
    Gopal, S
    Smirniotis, PG
    Gangoda, M
    Bose, RN
    MICROPOROUS AND MESOPOROUS MATERIALS, 2003, 60 (1-3) : 57 - 68
  • [10] Defect-designed ZSM-12 zeolites for alkylation of phenol with tert-butyl alcohol
    Liu, Baoyu
    Zhang, Jianwen
    Huang, Yeqing
    Xiong, Feng
    Luo, Rongchang
    MOLECULAR CATALYSIS, 2022, 519