4-(5-Bromo-2-hydroxyphenyl)but-3-ene-2-one

被引:1
作者
Zonouzi, Afsaneh [2 ]
Izakiana, Zakieh [2 ]
Rahmani, Hossein [3 ]
Ng, Seik Weng [1 ]
机构
[1] Univ Malaya, Dept Chem, Kuala Lumpur 50603, Malaysia
[2] Univ Tehran, Coll Sci, Dept Chem, Tehran, Iran
[3] Iranian Res Org Sci & Technol, Inst Ind Chem, Tehran, Iran
来源
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
关键词
D O I
10.1107/S1600536809009386
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The molecule of the title compound, C10H9BrO2, a doubly conjugated unsaturated ketone, is almost planar (r.m.s. deviation of the non-H atoms = 0.039 angstrom). In the crystal structure, two molecules are linked across a centre of inversion to form a hydrogen-bonded dimer by way of two O-H center dot center dot center dot O links.
引用
收藏
页码:O795 / U2338
页数:7
相关论文
共 8 条
[1]  
[Anonymous], 2008, APEX2 SAINT
[2]  
Barbour L.J., 2001, J SUPRAMOL CHEM, V1, P189, DOI [DOI 10.1016/S1472-7862(02)00030-8, 10.1016/S1472-7862(02)00030-8]
[3]   The reactivity of doubly-conjugated unsaturated ketones. Part III. Unsymmetrical hydroxy- and methoxy-derivatives. [J].
Buck, JS ;
Heilbron, IM .
JOURNAL OF THE CHEMICAL SOCIETY, 1922, 121 :1095-1101
[4]  
MARVEL CS, 1953, J ORG CHEM, V18, P1731
[5]  
Sheldrick G. M., 1996, Program for empirical adsorption correction of area detector data
[6]   A short history of SHELX [J].
Sheldrick, George M. .
ACTA CRYSTALLOGRAPHICA A-FOUNDATION AND ADVANCES, 2008, 64 :112-122
[7]  
Trost B.M, 1991, Comprehensive Organic Synthesis
[8]  
WESTRIP SP, 2009, PUBLCIF UNPUB