Status report on the Zagreb Radiocarbon Laboratory - AMS and LSC results of VIRI intercomparison samples

被引:25
作者
Sironic, Andreja [1 ]
Bronic, Ines Krajcar [1 ]
Horvatincic, Nada [1 ]
Baresic, Jadranka [1 ]
Obelic, Bogomil [1 ]
Felja, Igor [1 ]
机构
[1] Rudjer Boskovic Inst, Dept Expt Phys, Zagreb 10000, Croatia
关键词
Radiocarbon; Accelerator Mass Spectrometry (AMS); Graphite preparation; Radiocarbon Intercomparison (VIM);
D O I
10.1016/j.nimb.2012.01.048
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A new line for preparation of the graphite samples for C-14 dating by Accelerator Mass Spectrometry (AMS) in the Zagreb Radiocarbon Laboratory has been validated by preparing graphite from various materials distributed within the Fifth International Radiocarbon Intercomparison (VIRI) study. C-14 activity of prepared graphite was measured at the SUERC AMS facility. The results are statistically evaluated by means of the z-score and u-score values. The mean z-score value of 28 prepared VIRI samples is (0.06 +/- 0.23) showing excellent agreement with the consensus VIRI values. Only one sample resulted in the u-score value above the limit of acceptability (defined for the confidence interval of 99%) and this was probably caused by a random contamination of the graphitization rig. After the rig had been moved to the new adapted and isolated room, all u-score values laid within the acceptable limits. Our LSC results of VIRI intercomparison samples are also presented and they are all accepted according to the u-score values. (C) 2012 Elsevier B.V. All rights reserved.
引用
收藏
页码:185 / 188
页数:4
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