Synthesis, Crystal Structure and Biological activity of N-(5-(o-tolyl)-1,3,4-thiadiazol-2-yl)cyclopropanecarboxamide

被引:0
作者
Tong, Jian-Ying [1 ]
Sun, Na-Bo [1 ]
Wu, Hong-Ke [2 ]
Liu, Xing-Hai [2 ]
机构
[1] Zhejiang Shuren Univ, Coll Biol & Environm Engn, Hangzhou 310015, Zhejiang, Peoples R China
[2] Zhejiang Univ Technol, Coll Chem Engn & Mat Sci, Hangzhou 310014, Zhejiang, Peoples R China
来源
JOURNAL OF THE CHEMICAL SOCIETY OF PAKISTAN | 2013年 / 35卷 / 05期
基金
中国国家自然科学基金;
关键词
Crystal structure; synthesis; 1,3,4-thiadiazole; herbicidal activity; fungicidal activity; METAL-COMPLEXES; DERIVATIVES; MOIETY;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
A new 1, 3, 4-thiadiazole compound, N-(5-(o-tolyl)-1,3,4-thiadiazol-2-yl) cyclopropanecarboxamide, was synthesized and its structure was confirmed by H-1 NMR, MS and HRMS. The single crystal structure of the title compound was determined by X-ray diffraction. The preliminary biological test showed that the synthesized compound has moderate herbicidal activity against Brassica campestris and fungicidal activities against Sclerotinia sclerotiorum(Lib.) de Bary, Rhizoctonia solanii, Fusarium oxysporum, Corynespora cassiicola, and Botrytis cinerea.
引用
收藏
页码:1349 / 1353
页数:5
相关论文
共 16 条
[11]  
Tong JY, 2012, J CHEM SOC PAKISTAN, V34, P1300
[12]  
Turan N, 2010, J CHEM SOC PAKISTAN, V32, P630
[13]   Synthesis and Spectral Studies of Novel Co(II), Ni(II), Cu(II), Cd(II), and Fe(II) Metal Complexes with N-[5′-Amino-2,2′-bis(1,3,4-thiadiazole)-5-yl]-2-hydroxybenzaldehyde Imine (HL) [J].
Turan, Nevin ;
Sekerci, Memet .
SPECTROSCOPY LETTERS, 2009, 42 (05) :258-267
[14]  
Weng JQ, 2012, J CHEM SOC PAKISTAN, V34, P1248
[15]  
WILSON AJ, 1992, INT TABLE XRAY CRYST, VC
[16]  
Zhang ZQ, 2012, J CHEM SOC PAKISTAN, V34, P1048