Structural and optical properties of nanocrystalline lead sulfide thin films prepared by microwave-assisted chemical bath deposition

被引:25
|
作者
Obaid, A. S. [1 ,2 ]
Mahdi, M. A. [1 ,3 ]
Yusof, Y. [1 ]
Bououdina, M.
Hassan, Z. [1 ]
机构
[1] Univ Sains Malaysia, Sch Phys, Nanooptoelect Res & Technol Lab, Usm 11800, Penang, Malaysia
[2] Univ Anbar, Coll Sci, Dept Phys, Baghdad, Iraq
[3] Basrah Univ, Coll Sci, Dept Phys, Basrah, Iraq
关键词
Thin films; Chemical synthesis; Atomic force microscopy; X-ray diffraction; Optical properties; RAPID SYNTHESIS; HEATING METHOD; GROWTH;
D O I
10.1016/j.mssp.2013.02.005
中图分类号
TM [电工技术]; TN [电子技术、通信技术];
学科分类号
0808 ; 0809 ;
摘要
Nanocrystalline PbS thin films have been successfully deposited on glass substrate from lead nitrate (Pb2+ ions) and thiourea (S2- ions) precursors using MACB technique. The effects of molar concentration (0.02, 0.05, 0.075 and 0.1 M) on the structure and microstructure evolution were studied using X-ray diffraction (XRD), scanning electron microscopy, and atomic force microscopy. The optical properties were investigated using UV-vis spectrophotometer. Crystal size values obtained from XRD were compared with these calculated using atomic force microscopy (AFM). The values of optical band gaps were found to decrease as the ion source molar concentration increase. (C) 2013 Elsevier Ltd. All rights reserved.
引用
收藏
页码:971 / 979
页数:9
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