Synthesis of mesoporous titania thin films by a simple route at low-temperature via plasma treatment

被引:6
作者
Bian, Yurong [1 ,2 ]
Wang, Xiaohong [1 ,2 ]
Hu, Zhiyu [2 ,3 ]
机构
[1] Shanghai Univ, Dept Chem, Shanghai 200444, Peoples R China
[2] Shanghai Univ, Inst NanoMicroEnergy, Shanghai 200444, Peoples R China
[3] Shanghai Univ, Dept Phys, Shanghai 200444, Peoples R China
基金
中国国家自然科学基金;
关键词
OPTICAL-PROPERTIES; SILICA; TIO2; CALCINATION; REMOVAL; ANATASE; SURFACE; RUTILE;
D O I
10.1007/s10853-013-7221-0
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A new combination of techniques named evaporation-induced self-assembly-plasma etching (EISA-PE) method for mesoporous titania thin films preparation has been developed. The main advantage of this method is that the organic templates can be removed by plasma etching method thus the inorganic frameworks shrinkage or collapse induced by calcination can be avoided. Titania films prepared by this method have been characterized by Fourier transform infrared spectroscopy, thermogravimetric analyses, small and wide-angle X-ray diffraction, and field emission scanning electron microscope. The results show that titania thin film with well-resolved mesostructure can be created by EISA-PE method. The results also prove that plasma parameters have a great influence on the mesoporous property of the film and it is a good kind of catalyst support for methanol catalytic combustion.
引用
收藏
页码:4088 / 4096
页数:9
相关论文
共 50 条
[21]   Low-temperature ZrO2thin films obtained by polymeric route for electronic applications [J].
Boratto, Miguel H. ;
Lima, Joao V. M. ;
Scalvi, Luis V. A. ;
Graeff, Carlos F. O. .
JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS, 2020, 31 (18) :16065-16072
[22]   A Comparative Study on Photocatalytic Activity of Titania Nanowires Subjected to High-Temperature Calcination and Low-Temperature HCl Treatment [J].
Sun, Jing ;
Wu, Jin-Ming .
SCIENCE OF ADVANCED MATERIALS, 2013, 5 (06) :549-556
[23]   Synthesis of photocatalytic activity TiO2 thin films at low-temperature [J].
Zhao, WK ;
Fang, YL .
ACTA PHYSICO-CHIMICA SINICA, 2002, 18 (04) :368-371
[24]   Developments of Low-Temperature Solution Processing for Nanostructured Titania Dielectric Films [J].
Roy, Biplab K. ;
Zhang, Guangneng ;
Yoo, MoonHyo ;
Bae, In-Tae ;
Cho, Junghyun .
SCIENCE OF ADVANCED MATERIALS, 2010, 2 (01) :90-101
[25]   Synthesis of thin dense titania films via an aqueous solution-gel method [J].
Truijen, I. ;
Van Bael, M. K. ;
Van den Rul, H. ;
D'Haen, J. ;
Mullens, J. .
JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY, 2007, 41 (01) :43-48
[26]   Synthesis of thin dense titania films via an aqueous solution-gel method [J].
I. Truijen ;
M. K. Van Bael ;
H. Van den Rul ;
J. D’Haen ;
J. Mullens .
Journal of Sol-Gel Science and Technology, 2007, 41 :43-48
[27]   Low-temperature particle synthesis of titania/silica/natural rubber composites for antibacterial properties [J].
Wisutiratanamanee, Apisit ;
Poochinda, Kunakorn ;
Poompradub, Sirilux .
ADVANCED POWDER TECHNOLOGY, 2017, 28 (04) :1263-1269
[28]   Low-Temperature Sol-Gel Synthesis of Nanostructured Polymer/Titania Hybrid Films based on Custom-Made Poly(3-Alkoxy Thiophene) [J].
Niedermeier, Martin A. ;
Rawolle, Monika ;
Lellig, Philipp ;
Koerstgens, Volker ;
Herzig, Eva M. ;
Buffet, Adeline ;
Roth, Stephan V. ;
Gutmann, Jochen S. ;
Foerschl, Thomas ;
Huesing, Nicola ;
Mueller-Buschbaum, Peter .
CHEMPHYSCHEM, 2013, 14 (03) :597-602
[29]   Low temperature simple aqueous phase chemical synthesis and characterization of ZnO thin films [J].
Shinde, D. B. ;
Ghanwat, V. B. ;
Khot, K. V. ;
Kondalkar, V. V. ;
Mane, R. M. ;
Bagade, C. S. ;
Jagdale, S. K. ;
Mane, R. K. ;
Bhosale, P. N. .
MATERIALS TODAY-PROCEEDINGS, 2017, 4 (02) :119-125
[30]   Controllable synthesis of spindle-like ZnO nanostructures by a simple low-temperature aqueous solution route [J].
Lu, Hong-xia ;
Zhao, Yun-long ;
Yu, Xiu-jun ;
Chen, De-liang ;
Zhang, Li-wei ;
Xu, Hong-liang ;
Yang, Dao-yuan ;
Wang, Hai-long ;
Zhang, Rui .
APPLIED SURFACE SCIENCE, 2011, 257 (09) :4519-4523