A novel colorimetric probe derived from isonicotic acid hydrazide for copper (II) determination based on internal charge transfer (ICT)

被引：15
作者：
Liu, Qing [1 ]
Fei, Qiang [1 ]
Fei, Yanqun [2 ]
Fan, Qian [3 ]
Shan, Hongyan [1 ]
Feng, Guodong [1 ]
Huan, Yanfu [1 ]
机构：
[1] Jilin Univ, Coll Chem, Changchun 130023, Peoples R China
[2] Changchun Weiersai Biotec Pharmaceut Co Ltd, Changchun 130616, Peoples R China
[3] Changchun Vocat Inst Technol, Changchun 130033, Peoples R China
来源：
SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY | 2015年 / 151卷
基金：
中国国家自然科学基金;
关键词：
Isonicotic acid hydrazide; Colorimetric probe; Internal charge transfer (ICT); Copper determination; RATIOMETRIC FLUORESCENT-PROBE; PLASMA-MASS SPECTROMETRY; SCHIFF-BASE; CU-II; ON FLUORESCENT; ZN; PB; CD; CU(II); CHEMOSENSOR;
D O I：
10.1016/j.saa.2015.07.043
中图分类号：
O433 [光谱学];
学科分类号：
0703 ; 070302 ;
摘要：
A novel isonicotic acid hydrazide Schiff base derivative N'-(3,5-di-tert-butyl-2-hydroxy-benzylidene) isonicotinohydrazide (DHIH) has been synthesized and developed as a high selective and sensitive colorimetric probe for Cu2+ determination. Addition of Cu2+ to the solution of DHIH resulted in a rapid color change from colorless to yellow together with an obvious new absorption band appeared at the range of 400-440 nm by forming a 1:1 complex. Experimental results indicated that the DHIH could provide absorption response to Cu2+ with a linear dynamic range from 1.0 x 10(-5) to 1.0 x 10(-4) mol/L. The detection limit of Cu2+ was 5.24 x 10(-7) mol/L with good tolerance of other metal ions. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码：785 / 789
页数：5
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